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2 was by full-matrix least-squares techniques (SHELXL 93, G. M. Sheldrick, Universität Göttingen); all non-hydrogen atoms were refined anisotropically, and hydrongen atoms were included in calculated positions and allowed to ride on the relevant carbon atom. Final residuals wre R1 = 0.0969 for 4178 unique data with I>2σ(I) and wR2 = 0.3352 (qall data). Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100136. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: int. code +(1223) 336-033; e-mail: deposit@chemcrys.cam.ac.uk).
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