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Volumn 36, Issue 11, 1997, Pages 1215-1217

Lithiation of a Simple Amine with a Large Excess of n-Butyllithium: The Remarkable Product (Ph2NLi)·[Ph(C6H4Li)NLi] 2· (nBuLi)2·(Et2O)4

Author keywords

Amides; Lithiation; Lithium; Reaction mechanisms; Solid state structures

Indexed keywords


EID: 0030748529     PISSN: 05700833     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.199712151     Document Type: Article
Times cited : (39)

References (34)
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    • note
    • 2 was by full-matrix least-squares techniques (SHELXL 93, G. M. Sheldrick, Universität Göttingen); all non-hydrogen atoms were refined anisotropically, and hydrongen atoms were included in calculated positions and allowed to ride on the relevant carbon atom. Final residuals wre R1 = 0.0969 for 4178 unique data with I>2σ(I) and wR2 = 0.3352 (qall data). Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-100136. Copies of the data can be obtained free of charge on application to The Director, CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: int. code +(1223) 336-033; e-mail: deposit@chemcrys.cam.ac.uk).
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.