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note
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2 = 0.020 (0.015). All H atoms were idealized except the hydroxo-H atom whose coordinates and temperature factors were refined by full-matrix least-squares methods. The hexachlorocarborane anion in 1 was disordered over two sets of positions which was successfully modeled as a 0.88:0.12 disorder. Further details of the crystal structure investigations may be obtained from the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen (Germany), on quoting the depository numbers CSD-406151 and CSD-406152.
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