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84949159846
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Holland, B.C.; Gilman, N.W. Synth. Commun. 1974, 4, 203. A modified workup procedure was employed in which the use of 3N NaOH was omitted.
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0342373031
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13C NMR, IR and HRMS
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13C NMR, IR and HRMS.
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-
-
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18
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0001209154
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Buchwald, S.L; LaMarie, S.J.; Nielsen, R.B.; Watson, B.T.; King, S.M. Tetrahedron Lett. 1987, 28, 3895.
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19
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0342808040
-
-
note
-
6, 300 MHz) δ 0.75-1.05 (m, 15 H), 1.17 (d, 18 H, J= 7.5 Hz), 1.25-1.75 (m, 15 H), 5.90-6.05 (m, 2 H), 6.25 (dd, 1 H, J = 10, 15 Hz), 6.46 (d, 1 H, J = 18.5 Hz), 6.66 (dd, 1 H, J = 10, 18.5 Hz), 7.51 (dd, 1 H, J = 11.5, 15 Hz).
-
-
-
-
20
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0027441303
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Aldehyde 8 was also obtained using zirconocene chemistry via hydrozirconation of ethyl ethynyl ether according to Suzuki's protocol: Maeta, H.; Suzuki, K. Tetrahedron Lett. 1993, 34, 341.
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Maeta, H.1
Suzuki, K.2
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21
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0343242597
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Trienyl ester 3 was slightly unstable on silica gel, as were compounds 9, 12, and 4
-
Trienyl ester 3 was slightly unstable on silica gel, as were compounds 9, 12, and 4.
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-
-
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23
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0027997412
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Ley, S.V.; Norman, J.; Griffith, W.P.; Marsden, S.P. Synthesis 1994, 639.
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Synthesis
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Ley, S.V.1
Norman, J.2
Griffith, W.P.3
Marsden, S.P.4
-
24
-
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0342373029
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Stannane 4 was not obtained analytically pure due to its instability
-
Stannane 4 was not obtained analytically pure due to its instability.
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-
-
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25
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0027772653
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-
See, for example: Wipf, P.; Kim, Y.; Fritch, P. C. J. Org. Chem. 1993, 58, 7195. For reviews, see: Bestmann, H. J.; Vostrowski, O. Top. Curr. Chem. 1983, 109, 85. Maryanoff, B. E.; Reitz, A. B. Chem. Rev. 1989, 89, 863.
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J. Org. Chem.
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Wipf, P.1
Kim, Y.2
Fritch, P.C.3
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26
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0001956611
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-
See, for example: Wipf, P.; Kim, Y.; Fritch, P. C. J. Org. Chem. 1993, 58, 7195. For reviews, see: Bestmann, H. J.; Vostrowski, O. Top. Curr. Chem. 1983, 109, 85. Maryanoff, B. E.; Reitz, A. B. Chem. Rev. 1989, 89, 863.
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Top. Curr. Chem.
, vol.109
, pp. 85
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Bestmann, H.J.1
Vostrowski, O.2
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27
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0001848341
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-
See, for example: Wipf, P.; Kim, Y.; Fritch, P. C. J. Org. Chem. 1993, 58, 7195. For reviews, see: Bestmann, H. J.; Vostrowski, O. Top. Curr. Chem. 1983, 109, 85. Maryanoff, B. E.; Reitz, A. B. Chem. Rev. 1989, 89, 863.
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Maryanoff, B.E.1
Reitz, A.B.2
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