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Volumn 62, Issue 15, 1997, Pages 4912-4913

Stereo- and regiocontrolled synthesis of branched trisubstituted conjugated dienes by palladium(0)-catalyzed cross-coupling reaction

Author keywords

[No Author keywords available]

Indexed keywords

ALKADIENE; ALKENE; HALIDE;

EID: 0030743260     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo970647a     Document Type: Article
Times cited : (96)

References (22)
  • 1
    • 2042507954 scopus 로고
    • and references cited therein
    • (a) Miyaura, N.; Suzuki, A. Chem. Rev. 1995, 95, 2457-2483 and references cited therein.
    • (1995) Chem. Rev. , vol.95 , pp. 2457-2483
    • Miyaura, N.1    Suzuki, A.2
  • 9
    • 0001647908 scopus 로고
    • (a) For preparation of (Z)-vinyl iodide, see: Stork, G.; Zhao, K. Tetrahedron Lett. 1989, 30, 2173-2174.
    • (1989) Tetrahedron Lett. , vol.30 , pp. 2173-2174
    • Stork, G.1    Zhao, K.2
  • 11
    • 0001425048 scopus 로고
    • To our knowledge, comparison of the reactivity between (E)- and (Z)-vinyl iodides has been rarely documented, and we are aware of a single report where reactivity differences between (E)- and (Z)-vinyl bromides have been observed; see: Rossi, R.; Carpita, A. Tetrahedron Lett 1986, 27, 2529-2532.
    • (1986) Tetrahedron Lett , vol.27 , pp. 2529-2532
    • Rossi, R.1    Carpita, A.2
  • 17
    • 0000344537 scopus 로고
    • See Supporting Information for further details
    • Chiral internal alkynes 1a-1c were prepared from the corresponding dibromo olefins via the Corey-Fuchs protocol; see: Corey, E. J.; Fuchs, P. L. Tetrahedron Lett. 1972, 3769-3772. See Supporting Information for further details.
    • (1972) Tetrahedron Lett. , pp. 3769-3772
    • Corey, E.J.1    Fuchs, P.L.2
  • 18
    • 8544224067 scopus 로고    scopus 로고
    • note
    • 1H NMR (400 MHz).
  • 19
    • 8544263462 scopus 로고    scopus 로고
    • note
    • In this case, the coupling reaction was performed at room temperature for 15 h while an increase in the reaction temperature did not improve the yield of the desired coupling product.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.