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(a) Negishi, E.; Okukado, N.; King, A. O.; Van Horn, D. E.; Spiegel, B. I. J. Am. Chem. Soc. 1978, 100, 2254-2256.
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7
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(a) For preparation of (Z)-vinyl iodide, see: Stork, G.; Zhao, K. Tetrahedron Lett. 1989, 30, 2173-2174.
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Stork, G.1
Zhao, K.2
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11
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0001425048
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To our knowledge, comparison of the reactivity between (E)- and (Z)-vinyl iodides has been rarely documented, and we are aware of a single report where reactivity differences between (E)- and (Z)-vinyl bromides have been observed; see: Rossi, R.; Carpita, A. Tetrahedron Lett 1986, 27, 2529-2532.
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Rossi, R.1
Carpita, A.2
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0001209154
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(b) Buchwald, S. L.; La Maire, S. J.; Nielsen, R. B.; Watson, B. T.; King, S. M. Tetrahedron Lett. 1987, 28, 3895-3898.
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14
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0000395519
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Trost, B. M.; Fleming, I., Eds.; Pergamon: Oxford
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(a) Labinger, J. A. In Comprehensive Organic Synthesis; Hydrozirconation of C=C and C≡C and hydrometallation by other metals. Trost, B. M.; Fleming, I., Eds.; Pergamon: Oxford, 1991; Vol. 8, pp 667-702.
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17
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0000344537
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See Supporting Information for further details
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Chiral internal alkynes 1a-1c were prepared from the corresponding dibromo olefins via the Corey-Fuchs protocol; see: Corey, E. J.; Fuchs, P. L. Tetrahedron Lett. 1972, 3769-3772. See Supporting Information for further details.
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Corey, E.J.1
Fuchs, P.L.2
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18
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8544224067
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note
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1H NMR (400 MHz).
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19
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8544263462
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note
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In this case, the coupling reaction was performed at room temperature for 15 h while an increase in the reaction temperature did not improve the yield of the desired coupling product.
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20
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0025000356
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(a) Roush, W. R.; Moriarty, K. J.; Brown, B. B. Tetrahedron Lett. 1990, 31, 6509-6512.
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(b) Minato, A.; Suzuki, K.; Tamao, K. J. Am. Chem. Soc. 1987, 109, 1257-1258.
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Okukado, N.; Van Horn, D. E.; Klima, W. L.; Negishi, E. Tetrahedron Lett. 1978, 1027-1030.
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(1978)
Tetrahedron Lett.
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Okukado, N.1
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Klima, W.L.3
Negishi, E.4
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