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3042901142
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note
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A 300 W tungsten lamp with a cutoff filter was used. Characteristics of the cutoff filter: λ > 620 nm, transmittance - 83 % λ < 585 nm, transmittance < 1 %.
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85086527225
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note
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1H-NMR and mass spectra in agreement with the structure.
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31
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3042971759
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note
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The main byproduct is 5.5′-bisdodecylbisthiophene. Most of it can be easily removed since, in contrast with the product, it is not very soluble in hexane at-20 °C.
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