A new protocol for the removal of dimethoxytrityl ether groups derived from primary alcohols

Synthetic Communications

Volumn 27, Issue 22, 1997, Pages 3829-3833

  Wang, Yikang ^a   McGuigan, Christopher ^a  

^a CARDIFF UNIVERSITY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

ALCOHOL; ETHER DERIVATIVE;

REACTION ANALYSIS; REACTION TIME; REVIEW; SYNTHESIS; ULTRASOUND;

EID: 0030666257     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397919708005904     Document Type: Review

References (14)

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2. Weintraub, H.M. Sci. Am. 1990, 262, 40.
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4. Uhlmann, E.; Peymann, A. Chem. Rev. 1990, 90, 543.
5. Baertschi, A.J. Mol.Cell.Endocrinol. 1994, 101, R15.
6. Mason, W.P. IEEE Trans. Sonics Ultrason., SU-23 1976, 224.
7. Lickiss, P.L. and McGrath, V.E. Chem. Br. March, 1996, 47.
8. Richards, W.T. and Loomis, AlL. J. Am. Chem. Soc., 1927, 49, 3086.
9. Ley, S.V. and Low, C.M.R. "Ultrasound in Synthesis", Spring-Verlag: New York, 1989.
10. Han, B.H. and Boudjouk, P. J. Org. Chem.1982, 47, 5030.
11. Schmittling, E.A.; Sawyer, J.S. Tetrahedron Lett. 1991, 32, 7207.
12. Lee, A.S.Y.; Yeh, H.C.; Tsai, M.H. Tetrahedron Lett. 1995, 36, 6891.
13. Mason, T.J. [Ed.] Advances in Sonochemistry, 1990, 1, 1.
14. C (300 MHz, DMSO) 13.59 (s, 5-Me), 63.64 (C5'), 88.69 (C4'), 90.25 (C1'), 110.36 (C5), 127.37 (C2'), 136..34 (C3'), 138.17 (C6), 152.18 (C2), 165.25 (C4); the product was also identified by TLC comparison with an authentic sample. In the Table 'T' stands for thymine.