Optimal Detection of Weak nJ(1H-119Sn) Couplings by Gradient-Enhanced 1D and 2D Heteronuclear Multiple-Quantum Correlation Spectroscopy. Application to a Novel Tin Derivative of Erythromycin A

Journal of Magnetic Resonance

Volumn 124, Issue 1, 1997, Pages 218-222

  Martins, José C ^a   Kayser, François ^a,b   Verheyden, Patricia ^a   Gielen, Marcel ^a   Willem, Rudolph ^a   Biesemans, Monique ^a  

^a VRIJE UNIVERSITEIT BRUSSEL   (Belgium)

^b Goodyear Tech Res Ctr L ^*  (Luxembourg)

Author keywords

[No Author keywords available]

Indexed keywords

ERYTHROMYCIN; ERYTHROMYCIN ETHYLSUCCINATE; ORGANOTIN COMPOUND; S6 KINASE; TIN DERIVATIVE;

ARTICLE; ARTIFACT; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE; SYNTHESIS;

ARTIFACTS; ERYTHROMYCIN; ERYTHROMYCIN ETHYLSUCCINATE; NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; ORGANOTIN COMPOUNDS; RIBOSOMAL PROTEIN S6 KINASES; TIN COMPOUNDS;

EID: 0030622089     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.1996.1005     Document Type: Article

References (27)

1. M. Gielen, (Ed.), "Tin-Based Antitumour Drugs," Springer-Verlag, Berlin, 1990; M. Gielen, P. Lelieveld, D. de Vos, and R. Willem, in "Metal Complexes in Cancer Therapy" (B. K. Keppler, Ed.), p. 383, VCH, Weinheim, 1993.
2. M. Gielen, (Ed.), "Tin-Based Antitumour Drugs," Springer-Verlag, Berlin, 1990; M. Gielen, P. Lelieveld, D. de Vos, and R. Willem, in "Metal Complexes in Cancer Therapy" (B. K. Keppler, Ed.), p. 383, VCH, Weinheim, 1993.
3. C. Sanchez, F. Ribot, and S. Doeuff, in "Organometallic Polymers with Special Properties" (R. M. Lane, Ed.), p. 267, Kluwer Academic, New York, 1992.
4. W. R. Croasmun and R. M. K. Carlson (Eds.), "Two-Dimensional NMR Spectroscopy. Applications for Chemists and Biochemists," 2nd ed., VCH, New York, 1994.
5. J. T. B. H. Jastrzebski and G. Van Koten, Adv. Organometal. Chem. 35, 241 (1993).
6. E. R. T. Tiekink, Appl. Organometal. Chem. 5, 1 (1991).
7. E. R. T. Tiekink, Trends Organometal. Chem. 1, 71 (1994).
8. M. Gielen, A. El Khloufi, M. Biesemans, F. Kayser, R. Willem, B. Mahieu, D. Maes, J. N. Lisgarten, L. Wyns, A. Moreira, T. K. Chattopadhay, and R. A. Palmer, Organometallics 13, 2849 (1994).
9. F. Kayser, M. Biesemans, A. Delmotte, I. Verbruggen, B. Mahieu, I. De Borger, M. Gielen, R. Willem, and E. R. T. Tiekink, Organometallics 13, 4026 (1994).
10. F. Kayser, M. Biesemans, A. Delmotte, R. Hendrix, P. Malschaert, I. Verbruggen, B. Mahieu, R. Willem, and M. Gielen, Bull. Soc. Chim. Belges. 103, 273 (1994).
11. F. Kayser, M. Biesemans, M. Gielen, and R. Willem, J. Magn. Reson. A 102, 249 (1993).
12. F. Kayser, M. Biesemans, M. Gielen, and R. Willem, in "Advanced NMR Applications to Organometallic Chemistry," "Physical Organometallic Chemistry," Vol. 1, Chap. 3, Wiley, Chichester, 1996, in press.
13. F. Kayser, M. Biesemans, M. Bouâlam, E. R. T. Tiekink, A. El Khloufi, J. Meunier-Piret, A. Bouhdid, K. Jurkschat, M. Gielen, and R. Willem, Organometallics 13, 1198, 4126 (1994).
14. R. Willem, A. Bouhdid, F. Kayser, A. Delmotte, M. Gielen, J. C. Martins, M. Biesemans, B. Mahieu, and E. R. T. Tiekink, Organometallics 15, 1920 (1996).
15. M. Biesemans, R. Willem, S. Damoun, P. Geerlings, M. Lahcini, P. Jaumier, and B. Jousseaume, Organometallics 15, 2237 (1996).
16. R. Hurd and B. K. John, J. Magn. Reson. 91, 648 (1991).
17. O. Ruiz-Cabello, G. W. Vuister, C. T. Moonen, P. Van Gelderen, J. S. Cohen, and P. C. M. Van Zijl, J. Magn. Reson. 100, 342 (1992).
18. R. R. Ernst, G. Bodenhausen, and A. Wokaun, in "Principles of Nuclear Magnetic Resonance in One and Two Dimensions," p. 38, Oxford Univ. Press, Oxford, 1987.
19. J. Keeler, R. Clowes, A. L. Davis, and E. D. Laue, Methods Enzymol. 239, 145 (1994).
20. A. Bax, J. Magn. Reson. 52, 76 (1983).
21. A. Bax and M. F. Summers, J. Am. Chem. Soc. 109, 2093 (1986).
22. G. Davies, D. C. Kleinschmidt, P. R. Palan, and S. C. Virashtha, J. Chem. Soc. C, 3792 (1971).
23. J. Barber, J. I. Gyi, L. Lian, G. A. Morris, D. A. Pye, and J. K. Sutherland, J. Chem. Soc. Perkin Trans. 2, 1489 (1991).
24. J. R. Everett, E. Hunt, and J. W. Tyler, J. Chem. Soc. Perkin Trans. 2, 1481 (1991).
25. J. R. Everett and J. W. Tyler, J. Chem. Soc. Perkin Trans. 2, 1659 (1987).
26. B. Wrackmeyer, Annu. Rep. NMR Spectrosc. 16, 73 (1985).
27. J. C. Christofides and D. B. Davies, J. Am. Chem. Soc. 105, 5099 (1983).