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84920293807
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note
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3SH and black in the course of the reaction, presumably as a result of the formation of NiS.
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84920293806
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note
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3OH; Merck-Hitachi Pump L-7100; Knauer variable wavelength monitor) and identified by GC-MS (21), was 4.8 or 4.6 μmol, respectively.
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-
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36
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84920293805
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note
-
3 were found, as measured by HPLC (24) and determined by GC-MS (27), in addition to ∼25 μmol acetic acid.
-
-
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38
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84920293804
-
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note
-
2S, and the mixture was reacted at 120°C with silicone stoppers used to seal the reaction bottles.
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45
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84920293803
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note
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Supported by the Deutsche Forschungsgemeinschaft. We thank H. Simon and A. Bacher for providing the laboratory facilities and for their continued support, three unknown referees for suggestions, H. Krause and J. Winkler for assistance with mass spectroscopy, and O. Kandler for advice.
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