Metal polypyrazolylborates. X. Thienylmercury(II) derivatives: The X-ray crystal structure of [(5-Me)Thien-2-y1]Hg-( μ-Pz)2 b(Pz)2

Journal of Organometallic Chemistry

Volumn 515, Issue 1-2, 1996, Pages 213-220

  Gioia Lobbia, Giancarlo ^a   Cecchi, Patrizio ^b   Giordano, Federico ^c   Santini, Carlo ^a  

^a UNIVERSITY OF CAMERINO   (Italy)

^b UNIVERSITY OF TUSCIA   (Italy)

^c UNIVERSITY OF NAPLES FEDERICO II   (Italy)

Author keywords

199Hg NMR; Hg; Organomercury(II) compounds; Polypyrazolylborates; Thienylmercury(II) derivatives; X ray structure

Indexed keywords

EID: 0030607962     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/0022-328x(95)06098-h     Document Type: Article

References (28)

1. [1] S. Trofimenko, J. Am. Chem. Soc., 89 (1967) 3170.
2. [2] (a) S. Trofimenko, Acc. Chem. Res., 4 (1971) 17;
3. (b) S. Trofimenko, Chem. Rev., 72 (1972) 497.
4. [3] (a) S. Trofimenko, Prog. Inorg. Chem., 34 (1986) 115;
5. (b) K. Niedenzu and S. Trofimenko, Top. Curr. Chem., 131 (1986) 1.
6. [4] S. Trofimenko, Chem. Rev., 93 (1993) 943.
7. [5] (a) G. Gioia Lobbia, F. Bonati, P. Cecchi, A. Cingolani and A. Lorenzotti, J. Organomet. Chem., 378 (1989) 139;
8. (b) G. Gioia Lobbia, F. Bonati P. Cecchi and D. Leonesi, J. Organomet. Chem., 391 (1990) 155;
9. (c) G. Gioia Lobbia, F. Bonati P. Cecchi A. Lorenzotti and C. Pettinari, J. Organomet. Chem., 403 (1991) 317;
10. (d) G. Gioia Lobbia, P. Cecchi, R. Spagna, M. Colapietro, A. Pifferi and C. Pettinari, J. Organomet. Chem., 485 (1995) 45;
11. (e) G. Gioia Lobbia, P. Cecchi, S. Calogero, G. Valle, M. Chiarini and L. Stievano, J. Organomet. Chem., 503 (1995) 297.
12. (f) S. Calogero, L. Stievano, G. Gioia Lobbia, A. Cingolani, P. Cecchi and G. Valle, Polyhedron, 14 (1995) 1731.
13. [6] (a) G. Gioia Lobbia, F. Bonati, P. Cecchi and C. Pettinari, Gazz. Chim. Ital., 121 (1991) 355;
14. (b) G. Gioia Lobbia, P. Cecchi, F. Bonati and G. Rafaiani, Synth. React. Inorg. Met-Org. Chem., 22 (1992) 775;
15. (c) G. Gioia Lobbia, P. Cecchi, S. Bartolini, C. Pettinari and A. Cingolani, Gazz. Chim. Ital., 123 (1993) 641.
16. [7] Houben-Weyl: Methoden der organischen Chemie, Georg Thieme, Stuttgart, 1974, pp. 52-54.
17. [8] A.H. Cowley, C.J. Carrano, R.L. Geerts, R.A. Jones and C.M. Nunn, Angew. Chem. Int. Ed. Engl., 27 (1988) 277.
18. [9] A. Duatti, F. Tisato, F. Refosco, U. Mazzi and M. Nicolini, Inorg. Chem., 28 (1989) 4564.
19. [10] R.A. Kresinski, T.A. Hamor, L. Isam, C.J. Jones and J.A. McCleverty, Polyhedron, 8 (1989) 845.
20. [11] A.J. Canty, B.W. Skelton and A.H. White, Aust. J. Chem., 40 (1987) 1609.
21. [12] C. Lopez, R.M. Claramunt, D. Sanz, C. Foces Foces, F.H. Cano, R. Faure, E. Cayon and J. Elguero, Inorg. Chim. Acta, 176 (1990) 195.
22. [13] S. Aime, G. Digilio, R. Gobetto, P. Cecchi, G. Gioia Lobbia and M. Camalli, Polyhedron, 13 (1994) 2695.
23. [14] A.J. Canty, C.V. Lee, N. Chaichit and B.M. Gatehouse, Acta Crystallogr. Sect. B; 38 (1982) 743.
24. [15] A.J. Canty, N. Chaichit, B.M. Gatehouse, E.E. George and G. Hayhurst, Inorg. Chem., 20 (1981) 2414.
25. [16] N. Walker and D. Stuart, Acta Crystallogr. Sect. A; 39 (1983) 158.
26. [17] International Tables for X-ray Crystallography, Vol. IV, Kynoch, Birmingham, UK, 1984.
27. [18] Enraf-Nonius (1989) CAD-4 Software, Version 5.0, Enraf-Non-ius, Delft, Netherlands.
28. [19] G.M. Sheldrick, SHELX76 Program for Crystal Structure Determination, 1976, University of Cambridge, UK.