A one pot cobalt catalyzed regio- and stereoselective synthesis of oxazolidin-2-thiones from alkenes and trimethylsilylisothiocyanate

Tetrahedron Letters

Volumn 37, Issue 40, 1996, Pages 7315-7318

  Rajesh, S ^a   Reddy, M Madhava ^a   Iqbal, Javed ^a  

^a INDIAN INSTITUTE OF TECHNOLOGY KANPUR   (India)

Author keywords

[No Author keywords available]

Indexed keywords

2 OXAZOLIDINETHIONE DERIVATIVE; OXAZOLIDINE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CHIRALITY; DRUG SYNTHESIS; REACTION ANALYSIS; STEREOCHEMISTRY; X RAY ANALYSIS;

EID: 0030607162     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)01596-1     Document Type: Article

References (10)

1. 1. Hsiao, C. N.; Miller, M. J. J. Org. Chem., 1987, 52, 2201; Kazmierczak, F.; Helquist, P. J. J. Org. Chem., 1989, 54, 3988; Adamcrzyk, M; Mattingly, P. G.; Pan, Y. Tetrahedron Lett., 1995, 36, 5303.
2. 1. Hsiao, C. N.; Miller, M. J. J. Org. Chem., 1987, 52, 2201; Kazmierczak, F.; Helquist, P. J. J. Org. Chem., 1989, 54, 3988; Adamcrzyk, M; Mattingly, P. G.; Pan, Y. Tetrahedron Lett., 1995, 36, 5303.
3. 1. Hsiao, C. N.; Miller, M. J. J. Org. Chem., 1987, 52, 2201; Kazmierczak, F.; Helquist, P. J. J. Org. Chem., 1989, 54, 3988; Adamcrzyk, M; Mattingly, P. G.; Pan, Y. Tetrahedron Lett., 1995, 36, 5303.
4. 2 Beaupere, D.; El Meslouti, A.; Lelievre, Ph.; Uzan, R. Tetrahedron Lett., 1995, 36, 5347; Fernandez, J. M. G.; Mellet, C. O.; Fuentes, J. Tetrahedron Lett., 1992, 33, 3931; Grouiller, A.; Mackenzie, G.; Najib, B.; Shaw, G.; Ewing, D. J. Chem. Soc., Chem. Commun., 1988, 671.
5. 2 Beaupere, D.; El Meslouti, A.; Lelievre, Ph.; Uzan, R. Tetrahedron Lett., 1995, 36, 5347; Fernandez, J. M. G.; Mellet, C. O.; Fuentes, J. Tetrahedron Lett., 1992, 33, 3931; Grouiller, A.; Mackenzie, G.; Najib, B.; Shaw, G.; Ewing, D. J. Chem. Soc., Chem. Commun., 1988, 671.
6. 2 Beaupere, D.; El Meslouti, A.; Lelievre, Ph.; Uzan, R. Tetrahedron Lett., 1995, 36, 5347; Fernandez, J. M. G.; Mellet, C. O.; Fuentes, J. Tetrahedron Lett., 1992, 33, 3931; Grouiller, A.; Mackenzie, G.; Najib, B.; Shaw, G.; Ewing, D. J. Chem. Soc., Chem. Commun., 1988, 671.
7. 3 Punniyamurthy, T.; Bhatia, B.; Iqbal, J. J. Org. Chem., 1994, 59, 850. Reddy, M. M.; Punniyamurthy, T.; Iqbal, J. Tetrahedron Lett., 1995, 36, 159.
8. 3 Punniyamurthy, T.; Bhatia, B.; Iqbal, J. J. Org. Chem., 1994, 59, 850. Reddy, M. M.; Punniyamurthy, T.; Iqbal, J. Tetrahedron Lett., 1995, 36, 159.
9. 4. Iqbal, J., Pandey, A. Tetrahedron Lett., 1990, 31, 575.
10. 2 was added. Upon stirring for 2-3h, a pinkish brown powder precipitated from which the solvent was removed, dried and stored in desiccator. (See ref 3).