Debenzylation of complex oligosaccharides using ferric chloride

Tetrahedron Letters

Volumn 37, Issue 31, 1996, Pages 5477-5478

  Rodebaugh, Robert ^a   Debenham, John S ^a   Fraser Reid, Bert ^a  

^a DUKE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

OLIGOSACCHARIDE;

ARTICLE; CARBOHYDRATE SYNTHESIS; TECHNIQUE;

EID: 0030605827     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)01169-0     Document Type: Article

References (9)

1. 1. Greene, T.W., Wuts, P.G.M. Protective Groups in Organic Synthesis, 2nd ed, John Wiley & Sons: New York, 1991.
2. 2. Lerouge, P. Glycobiology 1994, 4, 127-134.
3. 3. Ikemoto, N.; Kim, O.K.; Lo, L.C.; Satyanarayana, V.; Chang, M.; Nakanishi, K. Tetrahedron Lett. 1992, 33, 4295-4298.
4. 4. a) Park, M.H.; Takeda, R.; Nakanishi, K. Tetrahedron Lett. 1987, 28, 3823-3824.
5. b) Kartha, K.P. R.; Dasgupta, F.; Singh, P.P.; Srivastava, H.C. J. Carbohydr. Chem. 1986, 5, 437.
6. 4, filtered, concentrated, and flash chromatographed on a silica column to give the desired product.
7. 3 with the acetylamido group.
8. 7. Kunz, H. ; Unverzagt, C. Angew. Chem. Int. Ed. Engl. 1988, 27, 1697-1699 and references therein.
9. 3 up to 7 h at 0 °C.