SCOPUS 정보 검색 플랫폼

Tetrahedron Letters

Volumn 37, Issue 35, 1996, Pages 6409-6412

Fragmentation of peroxyhemiacetals. Stereoselective synthesis of 1,2-dioxolanes

(4) Hernández, Rosendo a Velázquez, Silvia M a Suárez, Ernesto a Prangé, Thierry b

a INSTITUTO DE PRODUCTOS NATURALES Y AGROBIOLOGÍA (Spain)

b UNIVERSITÉ PARIS SACLAY (France)

Author keywords

[No Author keywords available]

Indexed keywords

1,2 DIOXOLANE DERIVATIVE; ACETAL DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; DRUG SYNTHESIS; REACTION ANALYSIS; STEREOCHEMISTRY; X RAY ANALYSIS;

EID: 0030603065 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/0040-4039(96)01360-3 Document Type: Article

Times cited : (10)

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- 13C-NMR) and analytical (HRMS) data in accord with the assigned structure.

49
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- note
- 4), filtered, and evaporated under reduced pressure. Rotative chromatography of the residue gave the crude acid that was treated with ethereal diazomethane, and purified. (6, 64% overall). Analogously, 5 gave dioxolane 7 in 61% yield.

50
- 85030276839
- note
- 1, Z = 4, a = 42.945(7), b = 14.524(3), and c = 5.973(2) Å, R(%) 8.8 for 2526 reflections with 1>3σ(I). Detailed X-ray crystallographic data are available, on request, from the Director, Cambrige Crystallographic Data Centre, 12 Union Road, Cambridge, CB2 1EZ, or as standard cif file from the authors at prange@lure.u-psud.fr.

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