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29
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0011906135
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note
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12. The corresponding syn diastereomer 22 provided an 83:17 mixture of diastereomers in the photocycloaddition. This ratio corresponds to that predicted by the molecular mechanics model. (formula presented)
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34
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0011896026
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note
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13C, and IR spectra as well as satisfactory combustion analyses or HRMS. All yields are for homogeneous, chromatographically pure products unless otherwise indicated.
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