Convenient synthesis of aromatic thiols from phenols

Tetrahedron Letters

Volumn 37, Issue 26, 1996, Pages 4523-4524

  Arnould, Jean Claude ^a   Didelot, Myriam ^a   Cadilhac, Caroline ^a   Pasquet, Marie Jeanne ^a  

^a Zeneca Pharma   (France)

Author keywords

[No Author keywords available]

Indexed keywords

PALLADIUM; PHENOL DERIVATIVE; THIOL DERIVATIVE;

ARTICLE; CATALYSIS; CHEMICAL REACTION; SYNTHESIS;

EID: 0030600178     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)00873-8     Document Type: Article

References (10)

1. 1. Wolan, Y. In The Chemistry of the Thiol Group,Vol. 1 ; Patai, S. Ed.; Wiley: London, 1974; pp 163-258.
2. 2. Barrett, G. C. Thiols in Comprehensive Organic Chemistry; Vol 3 Barton, D; Ollis, W. D. Ed; Jones, D. N. Pergamon Press pp. 10-11.
3. 3. Testaferri, L. ; Tingoli, M.; Tiecco, M. Tetrahedron Lett. 1980, 21, 3099-3100.
4. 4. Testaferri, L. ; Tiecco, M. ; Tingoli, M.; Chianelli, D.; Montanucci, M. Synthesis 1983, 751-755.
5. 5. Al-Kazimi, H. R.; Tarbell, D. S.; Plant, D. J. Am. Chem. Soc. 1955, 77, 2479-2482.
6. 6. Newman, M, S.; Karnes, H. A. J. Org. Chem. 1966, 31, 3980-3984.
7. 7. Rane, A. M.; Miranda, E. I.; Soderquist, J. A. Tetrahedron Lett. 1994, 35, 3225-3226.
8. 8. Ritter, K. Synthesis 1993, 735-762.
9. 9. Phillips, D.; O' Neill, B. T. Tetrahedron Lett. 1990, 31, 3291-3294.
10. 4, concentrated and purified by flash chromatography (AcOEt/hexane) to give the silylated thiol, which was deprotected in THF at 0°C, in the presence of TBAF.