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Volumn 37, Issue 52, 1996, Pages 9325-9328

Synthesis and self-association properties of diethynylbenzene macrocycles

Author keywords

[No Author keywords available]

Indexed keywords

BENZENE DERIVATIVE; MACROCYCLIC COMPOUND;

EID: 0030599667     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(97)82954-1     Document Type: Article
Times cited : (57)

References (31)
  • 1
    • 0001805503 scopus 로고
    • 1. a) Cram, D. J. Nature 1992, 356, 29-36.
    • (1992) Nature , vol.356 , pp. 29-36
    • Cram, D.J.1
  • 2
    • 0028236962 scopus 로고
    • b) Diederich, R Nature 1994, 369, 199-207.
    • (1994) Nature , vol.369 , pp. 199-207
    • Diederich, R.1
  • 8
    • 0001854116 scopus 로고
    • Stang, P. J.; Diederich, F. Eds.; VCH: Weinheim
    • h) Young, J. K.; Moore, J. S. in Modern Acetylene Chemistry; Stang, P. J.; Diederich, F. Eds.; VCH: Weinheim, 1995; p. 415-442.
    • (1995) Modern Acetylene Chemistry , pp. 415-442
    • Young, J.K.1    Moore, J.S.2
  • 14
    • 0020467141 scopus 로고
    • 6. Although it has been reported that oxidative coupling of 1,3-diethynylbenzene gave the parent hexamer 2(n= 1, X = Y = H), we were unable to reproduce the reaction; a) Ghose, B. N. J. Prakt. Chem. 1982, 324, 1052-1054.
    • (1982) J. Prakt. Chem. , vol.324 , pp. 1052-1054
    • Ghose, B.N.1
  • 21
    • 0011774558 scopus 로고    scopus 로고
    • note
    • 9 and (iv) deamination (56% for the 4 steps). Ethyl ester 6c was prepared by (i) monobromination of ethyl 4-aminobenzoate with NBS, (ii) iodination with IC1, and (iii) deamination (82% for the 3 steps).
  • 23
    • 0011711325 scopus 로고    scopus 로고
    • note
    • +].
  • 24
    • 0011713886 scopus 로고    scopus 로고
    • note
    • 2 = 173.9°).
  • 25
    • 0011744583 scopus 로고    scopus 로고
    • note
    • +].
  • 29
    • 0011745752 scopus 로고    scopus 로고
    • note
    • 15. We also prepared tetrakis-DBM having ethyl ester groups from 7c in a similar manner. However, we encountered difficulties in handling it because of its low solubility in most organic solvents.
  • 30
    • 33646891090 scopus 로고
    • We checked this assumption by Saunders-Hyne analysis. The monomer-dimer model gives the best fit over the full concentration range
    • 16. Saunders, M.; Hyne, J. B. J. Chem. Phys. 1958, 29, 1319-1323. We checked this assumption by Saunders-Hyne analysis. The monomer-dimer model gives the best fit over the full concentration range.
    • (1958) J. Chem. Phys. , vol.29 , pp. 1319-1323
    • Saunders, M.1    Hyne, J.B.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.