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21
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0011774558
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note
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9 and (iv) deamination (56% for the 4 steps). Ethyl ester 6c was prepared by (i) monobromination of ethyl 4-aminobenzoate with NBS, (ii) iodination with IC1, and (iii) deamination (82% for the 3 steps).
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22
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0000581214
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23
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0011711325
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note
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+].
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24
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0011713886
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note
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2 = 173.9°).
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25
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0011744583
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note
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+].
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26
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37049057697
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84987340550
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29
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0011745752
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note
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15. We also prepared tetrakis-DBM having ethyl ester groups from 7c in a similar manner. However, we encountered difficulties in handling it because of its low solubility in most organic solvents.
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30
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33646891090
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We checked this assumption by Saunders-Hyne analysis. The monomer-dimer model gives the best fit over the full concentration range
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16. Saunders, M.; Hyne, J. B. J. Chem. Phys. 1958, 29, 1319-1323. We checked this assumption by Saunders-Hyne analysis. The monomer-dimer model gives the best fit over the full concentration range.
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Saunders, M.1
Hyne, J.B.2
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