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85030198587
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note
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13C NMR, IR) and analytical (HRMS) data consistent with the assigned structure.
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31
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84942699384
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85030199452
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10. Obtained from Amano International Enzyme Co., Troy, VA.
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34
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85030203218
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note
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2 in the dark for 48 h at which time the reaction was judged to be at 50% completion. The mixture was filtered and the residue washed with methylene chloride. The solvent was removed in vacuo and the crude residue chromatographed (silica gel, hexanes/diethyl ether, 10:1) to afford (+)-4 (40 mg, 43%) and (-)-1 (35 mg, 44%).
-
-
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35
-
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85030203542
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note
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2
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37
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85030206233
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note
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2 (figure presented)
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39
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0001587357
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