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Volumn 37, Issue 43, 1996, Pages 7767-7770

Group transfer from silicon to carbon via tandem radical cyclizations of acylsilanes

Author keywords

[No Author keywords available]

Indexed keywords

SILANE DERIVATIVE;

EID: 0030597041     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)01773-X     Document Type: Article
Times cited : (22)

References (32)
  • 18
    • 85030271818 scopus 로고    scopus 로고
    • note
    • 8. Analyzed using a 3.3 mm × 2 m column packed with 10% SE-30 on Chromosorb W under a flow rate of 30 mL/min. Retention time (min) at column temperature = 130 °C: 7a = 6.3, 8a = 7.1, 9a = 7.9. Retention time (min) at column temperature = 140 °C: 7b = 8.5, 8b = 9.4, 9b = 10.5, 15 = 11.6, 18a = 7.8, 19a = 10.5, 20a = 9.4, 18b = 13.2, 19b = 16.0, 21 = 16.9.
  • 20
    • 0001496215 scopus 로고
    • (b) Wilt, J. W. Tetrahedron 1985, 41, 3979-4000.
    • (1985) Tetrahedron , vol.41 , pp. 3979-4000
    • Wilt, J.W.1
  • 23
    • 85030273871 scopus 로고    scopus 로고
    • note
    • 10. Acylsilane 15 was synthesized using methods similar to the synthesis of 6b as shown in scheme II. Instead of 1,5-dibromopentane, 1-bromopentane was used.
  • 24
    • 85030273408 scopus 로고    scopus 로고
    • note
    • 11. We did not determine the exact olefin geometry of 25a and 25b.
  • 27
    • 85030274722 scopus 로고    scopus 로고
    • note
    • 3) δ 12.7, 23.2, 25.0, 27.8, 29.6, 31.1, 33.7, 36.2, 47.1. 81.0 ppm.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.