Syntheses, structures and reactivities of [Os6Pd(CO)18(bipy)] and [{(bipy)Pd}2Os3(CO)12]: Crystal and molecular structures of [{(bipy)Pd}2(μ-H)(μ-CO)][H3Os4(CO)12] and [(C4H9)4N]2[Pd2I6]

Journal of Organometallic Chemistry

Volumn 510, Issue 1-2, 1996, Pages 219-231

  Chan, Suzanna ^a   Lee, Siu Ming ^a   Lin, Zhenyang ^b   Wong, Wing Tak ^a  

^a UNIVERSITY OF HONG KONG   (Hong Kong)

^b HONG KONG UNIVERSITY OF SCIENCE AND TECHNOLOGY   (Hong Kong)

Author keywords

Carbonyl; Clusters; Crystal structure; Osmium; Palladium

Indexed keywords

EID: 0030596360     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/0022-328X(95)05901-Z     Document Type: Article

References (59)

1. R.D. Adams and W. Wu, Organometallics, 12 (1993) 1248, and references cited therein.
2. R.D. Adams, J.E. Babin, R. Mathab and S. Wang, Inorg. Chem., 25 (1986) 1623, and references cited therein.
3. C. Couture and D.H. Farrar, J. Chem. Soc., Dalton Trans., (1987) 2245, 2253.
4. L.J. Farrugia, J.A.K. Howard, P. Mitrprachachon, J.L. Spencer, F.G.A. Stone and P. Woodward, J. Chem. Soc., Dalton Trans., (1981) 171.
5. L.J. Farrugia, J.A.K. Howard, P. Mitrprachachon, F.G.A. Stone and P. Woodward, J. Chem. Soc., Dalton Trans., (1981) 155, 162, 171.
6. E. Brivio, A. Ceriotti, R.D. Perogola, L. Garlaschelli, F. Demartin, M. Manassero, M. Sansoni, P. Zanello, F. Laschi and B.T. Heaton, J. Chem. Soc., Dalton Trans., (1994) 3237.
7. R.D. Adams, J.-C. Lii and W. Wu, Inorg. Chem., 31 (1992) 2556.
8. S. Chan and W.-T. Wong, J. Chem. Soc., Dalton Trans., (1994) 1605.
9. S. Chan and W.-T. Wong, J. Organomet. Chem., 489 (1995) C78.
10. R.J. Goudsmit, J.G. Jeffrey, B.F.G. Johnson, J. Lewis, R.C.S. McQueen, A.J. Sanders and J.-C. Liu, J. Chem. Soc., Chem. Commun., (1986) 24.
11. C.R. Eady, B.F.G. Johnson and J. Lewis, J. Chem. Soc., Dalton Trans., (1975) 2606.
12. A.J. Amoroso, B.F.G. Johnson, J. Lewis, C.K. Li, C.A. Morewood, P.R. Raithby, M.D. Vargas and W.T. Wong, J. Cluster Sci., 6 (1995) 163.
13. R. Goddard, P.W. Jolly, C. Krüger, K.-P. Schick and G. Wilke, Organometallics, 1 (1982) 1709.
14. R.D. Pergola, F. Demartin, L. Garlaschelli, M. Manassero, S. Martinengo, N. Masciocchi and M. Sansoni, Organometallics, 10 (1991) 2239.
15. R.D. Pergola, L. Garlaschelli, F. Demartin, M. Manassero and N. Masciocchi, J. Organomet. Chem., 436 (1992) 241.
16. B.F.G. Johnson, J. Lewis, W.J.H. Nelson, P. Puga, P.R. Raithby, D. Braga, M. McPartlin and W. Clegg, J. Organomet. Chem., 243 (1983) C13.
17. A. Fumagalli, G. Longoni, P. Chini, A. Albinati and S. Bruckner, J. Organomet. Chem., 202 (1980) 329.
18. D.M.P. Mingos, Acc. Chem. Res., 17 (1984) 311.
19. D.M.P. Mingos, J. Chem. Soc., Chem. Commun., (1983) 706.
20. W.-T. Wong, personal communication, 1989.
21. M.I. Bruce and B.K. Nicholson, Organometallics, 3 (1984) 101.
22. J.A.K. Howard, I.D. Salter and F.G.A. Stone, Polyhedron, 3 (1984) 567.
23. F. Maassarani, M. Pfeffer and G. Le Borgne, J. Chem. Soc., Chem Commun., (1987) 565.
24. F. Maassarani, M. Pfeffer and G. Le Borgne, Organometallics, 6 (1987) 2029.
25. D.F. Shriver, H.D. Kaesz and R.D. Adams, The Chemistry of Metal Cluster Complexes, VCH, Weinheim, 1990, p. 34.
26. E. Sappa, A. Tiripicchio and P. Braunstein, Coord. Chem. Rev., 65 (1985) 219.
27. F.A. Cotton, Prog. Inorg. Chem., 21 (1976) 1.
28. E.M. McGhee, B.M. Hoffman and J.A. Ibers, Inorg. Chem., 30 (1991) 2162.
29. J.-M. Barbe, P. Richard, M.A. Aukauloo, C. Lecomte, P. Petit and R. Guilard, J. Chem. Soc., Chem. Commun., (1994) 2757.
30. C.A. Hunter, Angew. Chem., Int. Edn. Engl., 32 (1993) 1584.
31. Z. Lin and M.B. Hall, Inorg. Chem., 30 (1991) 2569.
32. V.N. Zudin, V.D. Chinakov, V.M. Nekipelov, V.A. Likholobov and Y.I. Yermakov, J. Organomet. Chem., 289 (1985) 425.
33. A.R. Siedle, R.A. Newmark and W.B. Gleason, Inorg. Chem., 30 (1991) 2005.
34. M. Portnoy, F. Frolow and D. Milstein, Organometallics, 10 (1991) 3960.
35. M. Portnoy and D. Milstein, Oganometallics, 13 (1994) 600.
36. G. Minghetti, A.L. Bandini, G. Banditelli, F. Bonati, R. Szostak, C.E. Strouse, C.B. Knobler and H.D. Kaesz, Inorg. Chem., 22 (1983) 2332.
37. J.-C. Tsai, M.A. Khan and K.M. Nicholas, Organometallics, 10 (1991) 29; J.-C. Tsai, R.A. Wheeler, M.A. Khan and K.M. Nicholas, Organometallics, 10 (1991) 1344.
38. J.-C. Tsai, M.A. Khan and K.M. Nicholas, Organometallics, 10 (1991) 29; J.-C. Tsai, R.A. Wheeler, M.A. Khan and K.M. Nicholas, Organometallics, 10 (1991) 1344.
39. (a) J.N. Nicholls and M.D. Vargas, Inorg. Synth., 28 (1990) 234;
40. (b) J.N. Nicholls and M.D. Vargas, Inorg. Synth., 28 (1990) 238;
41. (c) J.N. Nicholls and M.D. Vargas, Inorg. Synth., 26 (1989) 295.
42. G.D. Smith, B.E. Hanson, J.S. Merola and F.J. Walles, Organometallics, 12 (1993) 568.
43. B.F.G. Johnson, J. Lewis, P.R. Raithby, G.M. Sheldrick and K. Wong, J. Chem. Soc., Dalton Trans., (1978) 673
44. (a) M.B. Hall and R.F. Fenske, Inorg. Chem., 11 (1972) 768;
45. (b) A.L. Sargent and M.B. Hall, Polyhedron, 9 (1990) 1977.
46. (a) R. Hoffmann, J. Chem. Phys., 39 (1963) 1397;
47. (b) R. Hoffmann and W.N. Lipscomb, J. Chem. Phys., 36 (1962) 2179, 3189; 37 (1962) 2872.
48. (b) R. Hoffmann and W.N. Lipscomb, J. Chem. Phys., 36 (1962) 2179, 3189; 37 (1962) 2872.
49. R.H. Summerville and R. Hoffmann, J. Am. Chem. Soc., 98 (1976) 7240.
50. Interactive MOPLOT: a package for the interactive display and analysis of molecular wavefunctions incorporating the program MOPLOT (D. Lichtenburger), PLOTDEN (R.F.W. Bader, D.J. Kenworthy, P.M. Beddal, G.R. Runtz and S.G. Anderson), SCHUSS (R.F.W. Bader, G.R. Runtz, S.G. Anderson and F.W. BieglerKoenig) and EXTREM (R.F.W. Bader and F.W. Biegler-Koenig), P. Sherwood and P.J. MacDougall, 1989.
51. A.C.T. North, D.C. Phillips and F.S. Mathews, Acta Crystallogr., Sect. A, 24 (1968) 351.
52. (a) D.T. Cromer and J.T. Waber, International Tables for X-ray Crystallography, Vol. 4, Kynoch, Birmingham, 1974, Table 2.2B;
53. (b) D.T. Cromer and J.T. Waber, International Tables for X-ray Crystallography, Vol. 4, Kynoch, Birmingham, 1974, Table 2.3.1.
54. P. Main, S.J. Fiske, S.E. Hill, L. Lessinger, G. Germain, J.-P. Declercq and M.M. Wolfcon, MULTAN 80, A System of Computer Programs for the Automatic Solution of Crystal Structures from X-ray Diffraction Data, University of York, York, University of Louvain, Louvain, 1980.
55. M.C. Burla, M. Camalli, G. Cascarano, C. Giacovazzo, G. Polidor, R. Spagna and D. Viterbo, J. Appl. Crystallogr., 22 (1989) 389.
56. H.-F. Fan, Structure Analysis Programs with Intelligent Control, Rigaku Corporation, Tokyo, 1990.
57. H.-F. Fan, Structure Analysis Programs with Intelligent Control, Rigaku Corporation, Tokyo, 1991.
58. SDP Structure Determination Package, Enraf-Nonius, Delft, 1985.
59. TeXsan: Crystal Structure Analysis Package, Molecular Structure Corporation, 1985, 1992.