Synthesis and properties of dialkyl derivatives of di[60]fullerenylbutadiyne and di[60]fullerenylacetylene: The buckydumbbells

Tetrahedron Letters

Volumn 37, Issue 34, 1996, Pages 6153-6156

  Komatsu, Koichi ^a   Takimoto, Naohiko ^a   Murata, Yasujiro ^a   Wan, Terence S M ^b   Wong, Thomas ^b  

^a KYOTO UNIVERSITY   (Japan)

^b HONG KONG UNIVERSITY OF SCIENCE AND TECHNOLOGY   (Hong Kong)

Author keywords

[No Author keywords available]

Indexed keywords

ACETYLENE; BUTADIENE DIEPOXIDE;

ARTICLE; ELECTRON; MOLECULAR INTERACTION; SYNTHESIS;

EID: 0030593626     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)01335-4     Document Type: Article

References (16)

1. 1. a) An, Y.-Z.; Rubin, Y.; Schaller, C.; McElvany, S. W. J. Org. Chem. 1994, 59, 2927-2929.
2. b) Andersen, H. L.; Faust, R.; Rubin, Y.; Diederich, F. Angew. Chem., Int. Ed. Eng. 1994, 33, 1366-1368.
3. c) Isaacs, L.; Seiler, P.; Diederich, F. Angew. Chem., Int. Ed. Eng. 1995, 34. 1466-1469. Timmerman, P.; Anderson, H. L.; Faust, R.; Nierengarten, J.-F.; Habicher, T.; Seiler, P.; Diederich, F. Tetrahedron, 1996, 52, 4925-4947.
4. c) Isaacs, L.; Seiler, P.; Diederich, F. Angew. Chem., Int. Ed. Eng. 1995, 34. 1466-1469. Timmerman, P.; Anderson, H. L.; Faust, R.; Nierengarten, J.-F.; Habicher, T.; Seiler, P.; Diederich, F. Tetrahedron, 1996, 52, 4925-4947.
5. 2. Komatsu, K.; Murata, Y.; Takimoto, N.; Mori, S.; Sugita, N.; Wan, T. S. M. J. Org. Chem. 1994, 59, 6101-6102. The same compound 2 was independently synthesized by Diederich et al (Ref. 1b).
6. 3. a) Kitagawa, T.; Tanaka, T.; Takata, Y.; Takeuchi, K.; Komatsu, K. J. Org. Chem. 1995, 60, 1490-1491.
7. b) Murata, Y; Komatsu, K.; Wan, T. S. M. Tetrahedron, 1996, 52, 5077-5090.
8. 60H ( Keshavarz-K, M.; Knight, B.; Srdanov, G.; Wudl, F. J. Am. Chem. Soc. 1995, 117, 11371-11372).
9. 60H ( Keshavarz-K, M.; Knight, B.; Srdanov, G.; Wudl, F. J. Am. Chem. Soc. 1995, 117, 11371-11372).
10. 60H ( Keshavarz-K, M.; Knight, B.; Srdanov, G.; Wudl, F. J. Am. Chem. Soc. 1995, 117, 11371-11372).
11. max 211 nm, 258, 312, 434, 700.
12. max 219 nm (log ε 5.18), 256 (5.03), 436 (3.76), 457sh (3.68), 689 (2.54).
13. 7. Prato, M.; Suzuki, T.; Wudl, F. J. Am. Chem. Soc. 1993, 115, 7876-7877.
14. 8. a) Adams, R. N. Electrochemistry at Solid Electrodes 1969, Marcel Dekker, Inc., New York, pp. 143-158.
15. 5) was recently reported by Diederich and coworkers in a completely independant study: Timmerman, P.; Witschel, L. E.; Diederich, F.; Boudon, C.; Gisselbrecht, J.-P.; Gross, M. Helv. Chim. Acta 1996, 79, 6-20.
16. 5) was recently reported by Diederich and coworkers in a completely independant study: Timmerman, P.; Witschel, L. E.; Diederich, F.; Boudon, C.; Gisselbrecht, J.-P.; Gross, M. Helv. Chim. Acta 1996, 79, 6-20.