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37
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note
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2, followed by addition of 150 mg triphosgene (0.5 mmol), 100 μL dry DMF and a catalytic amount of tetrabutylammonium chloride. After completion of the reaction (1 h), as was demonstrated by TLC, the reaction mixture was filtrated over a small amount of silica 60 (eluent: EtOAc/hexanes, 1/3, v/v) and the solvent evaporated affording sulfonylchloride 9c in a yield of 94% (198 mg).
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