Synthesis, redox chemistry and solid state structure of di- and trinuclear ferrocenyl substituted N-alkylpyrazolyl pyridine complexes

Journal of Organometallic Chemistry

Volumn 514, Issue 1-2, 1996, Pages 137-147

  Thiel, Werner R ^a   Priermeier, Thomas ^a   Fiedler, Dirk A ^a   Bond, Alan M ^b   Mattner, Mike R ^a  

^a TECHNICAL UNIVERSITY OF MUNICH   (Germany)

^b MONASH UNIVERSITY   (Australia)

Author keywords

Carbonyl complexes; Cyclovoltammetry; Ferrocene; X ray structure

Indexed keywords

EID: 0030591568     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/0022-328X(95)06028-U     Document Type: Article

References (38)

1. [1] A. Togni and T. Hayashi (eds.), Ferrocenes, VCH, Weinheim, 1995, pp. 105-168.
2. [2] (a) W. Kaim and B. Schwerderski, Bioanorganische Chemie, B.G. Teubner, Stuttgart, 1991;
3. (b) R. Hahn, Ph. D. Thesis, Technical Univesity of Munich, 1994.
4. [3] (a) U. Siemeling, U. Vorfeld, B. Neumann and H.-G. Stammler, Chem. Ber., 128 (1995) 481;
5. (b) I.R. Butler, Organometallics, 11 (1992) 74;
6. (c) F. Gelin and R.P. Thummel, J. Org. Chem., 57 (1992) 3780;
7. (d) I.R. Butler, S.J. McDonald, M. Hursthouse and K.M. Abdul Malik, Polyhedron, 14 (1995) 529;
8. (e) B. Farlow, T.A. Nile, J.L. Walsh and A.T. McPhail, Polyhedron, 12 (1993) 2891;
9. (f) I.R. Butler and J.-L. Roustan, Can. J. Chem., 68 (1990) 2212;
10. (g) F. Jäkle, T. Priermeier and M. Wagner, Chem. Ber., 128 (1995) 1163.
11. [4] H. Brunner and T. Scheck, Chem. Ber., 125 (1992) 701.
12. [5] (a) W.R. Thiel, M. Angstl and T. Priermeier, Chem. Ber., 127 (1994) 2373;
13. (b) W.R. Thiel, M. Angstl and N. Hansen, J. Mol. Catal., A103 (1995) 5;
14. (c) W.R. Thiel and T. Priermeier, Angew. Chem., 107 (1995) 1870; W.R. Thiel and T. Priermeier, Angew. Chem. Int. Ed. Engl., 34 (1995) 1737.
15. (c) W.R. Thiel and T. Priermeier, Angew. Chem., 107 (1995) 1870; W.R. Thiel and T. Priermeier, Angew. Chem. Int. Ed. Engl., 34 (1995) 1737.
16. [6] L. Wolf and H. Hennig, Z. Anorg. Allg. Chem., 341 (1965) 1.
17. [7] (a) H. tom Dieck and E. Kühl, Z. Naturforsch, b, 37 (1982) 324;
18. (b) J.W. Hershberger, R.J. Klingler and J.K. Kochi, J. Am. Chem. Soc., 104 (1982) 3034.
19. [8] L.C. Behr, R. Fusco and C.H. Jarboe, in R.H. Wiley (ed.), The Chemistry of Heterocyclic compounds - Pyrazoles, Pyrazolines, Pyrazolidines, Indazoles and Condensed Rings, Interscience, New York, 1967, pp. 10-62.
20. [9] D.J. Darensbourg and R.L. Kump, Inorg. Chem., 17 (1978) 2680.
21. [10] L.M. Haines and M.H.B. Stiddard, Adv. Inorg. Radiochem., 12 (1969) 53.
22. [11] B.M. Foxman, D.D. Gronbeck and M. Rosenblum, J. Organomet. Chem., 413 (1991) 287.
23. [12] R.R. Ernst, G. Bodenhausen and A. Wokaun, Principles of Nuclear Magnetic Resonance in One and Two Dimensions, Clarendon, Oxford, 1987.
24. [13] G.C. Levy, Tetrahedron Lett., 35 (1972) 3709.
25. [14] For example: (a) D. Osella, L. Milone, C. Nervi and M. Ravera, J. Organomet. Chem., 488 (1995) 1;
26. (b) E.E. Bunel, L. Valle, N.L. Jones, P.J. Carroll, C. Barra, M. Gonzalez, N. Munoz, G. Visconti, A. Aizman and J.M. Manriquez, J. Am. Chem. Soc., 110 (1988) 6596;
27. (c) T.-Y. Dong, C.-H. Huang, C.-K. Chang, H.-C. Hsieh, S.-M. Peng and G.-H. Lee, Organometallics, 14 (1995) 1776;
28. (d) D. Astruc, Chem. Rev., 88 (1988) 1189.
29. [15] H. Plenio, J. Yang, R. Diodone and J. Heintze, Inorg. Chem., 33 (1994) 4098.
30. [16] R.J. Crutchley and A.B.P. Lever, Inorg. Chem., 21 (1982) 2276.
31. [17] International Tables of Crystallography, Vol. I, Kynoch, Birmingham, 1974.
32. [18] A.L. Spek, The EUCLID package, in D. Sayre (ed.), Computational Crystallography, Clarendon, Oxford, 1982, p. 528.
33. [19] (a) E.O. Schlemper, G.N. Schrauzer and L.A. Hughes, Polyhedron, 3 (1984) 377;
34. (b) W.A. Herrmann, W.R. Thiel, J.G. Kuchler, J. Behm and E. Herdtweck, Chem. Ber., 123 (1990) 1963.
35. [20] (a) P.J. Graham, R.V. Lindsey, G.W. Parshall, M.L. Peterson and G.M. Whitman, J. Am. Chem. Soc., 79 (1957) 3416;
36. (b) R.B. Woodward, M. Rosenblum and M. Whiting, J. Am. Chem. Soc., 74 (1952) 3458.
37. [21] G.M. Sheldrick, SHELXS-86, Program for Structure Refinement, University of Göttingen, Göttingen, 1986.
38. [22] D.J. Watkin, P.W. Betteridge and J.R. Carruthers, CRYSTALS User Manual, Oxford University Computing Laboratory, Oxford, 1986.