New synthesis of phenyl-substituted 2,3-dihydro-1,3-dithiolo[4,5-e][1,4]dithiin-6-thione

Tetrahedron Letters

Volumn 37, Issue 42, 1996, Pages 7603-7606

  Noh, Dong Youn ^a   Lee, Ha Jin ^a   Hong, Jongki ^b   Underhill, Allan E ^c  

^a Seoul Women University   (South Korea)

^b Korea Basic Science Institute (KBSI)   (South Korea)

^c BANGOR UNIVERSITY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

1,3 DITHIOLE DERIVATIVE; 1,4 DITHIANE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; REACTION ANALYSIS; STEREOCHEMISTRY; X RAY CRYSTALLOGRAPHY;

BETULACEAE;

EID: 0030583502     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)01672-3     Document Type: Article

References (19)

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16. 3. Full matrix least-squares refinement yields the final R value of 0.0664 (wR = 0.1696) for 5963 independent reflections [3.24° ≤ 2θ ≤ 50.02°, I 〉 2σ(I)]. The crystal structures were determined by the direct method using SHELXS-86 and SHELXL-93, and measured on an Enraf-Nonius CAD-4 diffractometer at 293(2)K using graphite-monochromated molybdenum radiation (λ = 0.71073Å) and ω-2θ scan mode. Atomic coordinates and e.s.d.'s have been deposited at the Cambridge Crystallographic Data Center.
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