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(e) T.G. Traylor, T. Nakano, B.E. Dunlap, P.S. Traylor and D. Dolphin, J. Am. Chem. Soc., 108 (1986) 2782.
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[7] E.N. Jacobsen, W. Zhang, L.C. Muci, J.R. Ecker and L. Deng, J. Am. Chem. Soc., 113 (1991) 7063.
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[8] R. Hage, J.E. Iburg, J. Kerschner, J.H. Koek, E.L.M. Lempers, R.J. Martens, U.S. Racherla, S.W. Russell, T. Swarthoff, M.R.P. van Vliet, J.B. Warnaar, L. van der Wolf and B. Krijnen, Nature, 369 (1994) 637.
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30144437908
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2 mixtures show a resonance at δ = 1.33 ppm, which has previously been ascribed to 2-hydroxy-2-hydroperoxypropane [10]. There is no evidence for the formation of dimethyldioxirane in reaction conditions. Moreover, no products are formed at all when the Mn catalyst is omitted from the reaction mixture, whereas dimethyldioxirane is known to epoxidize olefins spontaneously. For NMR spectra and reactivity of dimethyldioxirane: R.W. Murray and R. Jeyaraman, J. Org. Chem., 50 (1985) 2847.
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5COOH group: S. Banfi, F. Legranmandi, F. Montanari, G. Pozzi and S. Quici, J. Chem. Soc. Chem. Commun., (1991) 1285.
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(b) K. Wieghardt, U. Bossek, B. Nuber, J. Weiss, J. Bonvoisin, M. Corbella, S.E. Vitols and J.J. Girerd, J. Am. Chem. Soc., 110 (1988) 7398.
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26
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0011492604
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note
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3 is used as a catalyst, nor when another solvent is used.
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30
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0001338714
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[16] A.A. Belal, P. Chaudhuri, I. Fallis, L.J. Farrugia, R. Hartung, N.M. McDonald, B. Nuber, R.D. Peacock, J. Weiss and K. Wieghardt, Inorg. Chem., 30 (1991) 4397.
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31
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[17] (a) R.S. Czernuszewicz, Y.O. Su, M.K. Stern, K.A. Macor, D. Kim, J.T. Groves and T.G. Spiro, J. Am. Chem. Soc., 110 (1988), 4158;
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[18] K. Wieghardt, U. Bossek, P. Chaudhuri, W. Herrmann, B.C. Mehnke and J. Weiss, Inorg. Chem., 21 (1982) 4308.
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[19] (a) K. Wieghardt, W. Schmidt, B. Nuber and J. Weiss, Chem. Ber., 112 (1979) 2228;
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