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85033031283
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note
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19
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17
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0024972656
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0 alkylidenes has been recently addressed: Schlund, R.; Schrock, R. R.; Crowe, W. E. J. Am. Chem. Soc. 1989, 111, 8004. Also see: Schrock, R. R.; McConville, D.; Oskam, J.; O'Dell, R.; Hofmeister, G.; Luo, S.; Zanetti, N. Abstracts of Papers, 208th National Meeting of the American Chemical Society, Washington, DC, Aug 1994; American Chemical Society: Washington, DC, 1994; POLY 356.
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Grubbs, R.H.1
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18
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0024733498
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0 alkylidenes has been recently addressed: Schlund, R.; Schrock, R. R.; Crowe, W. E. J. Am. Chem. Soc. 1989, 111, 8004. Also see: Schrock, R. R.; McConville, D.; Oskam, J.; O'Dell, R.; Hofmeister, G.; Luo, S.; Zanetti, N. Abstracts of Papers, 208th National Meeting of the American Chemical Society, Washington, DC, Aug 1994; American Chemical Society: Washington, DC, 1994; POLY 356.
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Schlund, R.1
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19
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3042955307
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Abstracts of Papers, Washington, DC, Aug American Chemical Society: Washington, DC, 1994; POLY 356
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0 alkylidenes has been recently addressed: Schlund, R.; Schrock, R. R.; Crowe, W. E. J. Am. Chem. Soc. 1989, 111, 8004. Also see: Schrock, R. R.; McConville, D.; Oskam, J.; O'Dell, R.; Hofmeister, G.; Luo, S.; Zanetti, N. Abstracts of Papers, 208th National Meeting of the American Chemical Society, Washington, DC, Aug 1994; American Chemical Society: Washington, DC, 1994; POLY 356.
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20
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0000676127
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0 rhenium alkylidyne-mediated metathesis reaction with 2-butyne has been reported: Weinstock, I. A.; Schrock, R. R.; Davis, W. M. J. Am. Chem. Soc. 1991, 113, 135.
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0002591778
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24
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0001077422
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25
-
-
85033009554
-
-
note
-
2O. At 25 °C, 12 μL (0.128 mmol) of tert-butylphosphaacetylene (1) was added and the vial was capped; the catalyst solution changed from yellow to red-orange. After it was stirred for 5 h, solvent removal under vacuum left an orange residue which was dissolved in a minimum of dry pentane. Cooling at -40 °C yielded 0.075 g of orange crystals (87% yield based on starting molybdenum alkylidene 2).
-
-
-
-
26
-
-
85033003326
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-
note
-
12PMo: C, 44.84; H, 5.27; N, 1.74. Found: C, 45.05; H, 5.19; N, 1.79.
-
-
-
-
27
-
-
85033009362
-
-
note
-
2. All crystallographic calculations were performed using the UCI-modified version of the UCLA Crystallographic Computing Package (UCLA Crystallographic Computing Package, University of California, Los Angeles, 1981: Strouse, C. Personal communication) and the SHELXTL PLUS program set (PC version: Sheldrick, G. SHELX-TL PLUS program set; Siemens Analytical X-Ray Instruments: Madison, WI, 1990).
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30
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1942540388
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0002714978
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0000074697
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