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PBO and PBT fiber described in this paper were not heat treated unless specified. Strong ESR signals identical to those observed for as spun fibers were also observed for heat-treated PBO and PBT fiber prepared at Dow and a heat-treated PBT fiber sample prepared by dnPont. ESR experiments for heat-treated fibers were performance in air only.
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note
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Numbers are absolute pressures which are gauge pressures plus 14.7 psi.
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For unclear reasons, excess DADHB is required to completely convert the carboxylic acid to benzoxazole. This is not true for 12, a similar PBT model compound.
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