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2. (a) Schlosser, M. In Organometallics in Syntheses; Schlosser, M., Ed.; J. Wiley & Sons: Chichester, 1994; pp. 47-50.
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(b) Schölkopff, U. In Houben-Weyl, Methoden der Organischen Chemie, Band 13/I; G. Thieme Verlag: Stuttgart, 1970; pp. 127-133. (c) Ref. 1, pp. 47-49. (d) Shapiro, R. H. Org. React. 1976, 23, 405-507.
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5. For another methodology based on arene-catalysed lithiation reactions of allylic and benzylic alcohols or their silylated derivatives, see: Alonso, E.; Guijarro, D.; Yus, M. Tetrahedron 1995, 51, 11457-11464.
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(b) Guijarro, D.; Guillena, G.; Mancheño, B.; Yus, M. Tetrahedron 1994, 50, 3427-3436.
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7. Guijarro, D.; Mancheño, B.; Yus, M. Tetrahedron 1994, 50, 8551-8558.
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8. For the last paper from our laboratory on the use of the arene-catalysed lithiation, see: Guijarro, A.; Ortiz, J.; Yus, M. Tetrahedron Lett. 1996, 37, 5597-5600.
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10. Anderson, B. A.; Bao, J.; Brandvold, T. A.; Challener, C. A.; Wulff, W. D.; Xu, Y.-C.; Rheingold, A. L. J. Am. Chem. Soc. 1993, 115, 10671-10687.
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85136556023
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3 (1.2 mmol) was added to the reaction mixture before the addition of this reagent and benzaldehyde, and the temperature was allowed to rise to 20°C before the final hydrolyses
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3 (1.2 mmol) was added to the reaction mixture before the addition of this reagent and benzaldehyde, and the temperature was allowed to rise to 20°C before the final hydrolyses.
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