Cp*AlR2 compounds (R = Me, Et, iBu): Synthesis and structure of novel aluminium organyls with a pentamethylcyclopentadienyl substituent as well as structure of analogous Cp′AlR2 compounds (Cp′ = Cp, MeCp; R = Me, Et)

Journal of Organometallic Chemistry

Volumn 513, Issue 1-2, 1996, Pages 135-138

  Scherer, Markus ^a,b   Kruck, Thomas ^a  

^a UNIVERSITY OF COLOGNE   (Germany)

^b UNIVERSITY OF TEXAS AT AUSTIN   (United States)

Author keywords

(Cyclopentadienyl)aluminium complexes; Organoaluminium compounds; Pentamethylcyclopentadienyl ligand

Indexed keywords

EID: 0030567469     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/0022-328X(95)05925-F     Document Type: Article

References (20)

1. [1] C. Dohmeier, C. Robl, M. Tacke and H. Schnöckel, Angew. Chem., 103 (1991) 594.
2. [2] S. Schulz, H.W. Roesky, H.J. Koch, G.M. Sheldrick, D. Stalke and A. Kuhn, Angew. Chem., 105 (1993) 1828.
3. [3] H.J. Koch, S. Schulz, H.W. Roesky, M. Noltemeyer, H.G. Schmidt, A. Heine, R. Herbst-Irmer, D. Stalke and G.M. Sheldrick, Chem. Ber., 125 (1992) 1107.
4. [4] N. Giannini and S. Cesca, Gazz. Chim. Ital., 91 (1961) 597.
5. [5] P.R. Schonberg, R.T. Paine, C.F. Campana and E.N. Duesler, Organometallics, 1 (1982) 799.
6. [6] R. Benn, E. Janssen, H. Lehmkuhl and A. Rufinska, J. Organomet. Chem., 333 (1987) 155.
7. [7] J.D. Fischer, M.Y. Wei, R. Willett and P.J. Shapiro, Organometallics, 13 (1994) 3324.
8. [8] W. Ziemkowska, S. Pasynkiewicz and E. Kalbarczyk, J. Organomet. Chem., 465 (1994) 93; L.A. Nekhaeva, G.N. Bondarenko, S.V. Rykov, A.I. Nekhaev, B.A. Krentsel, V.P. Mar'in, L.I. Vyshinskaya, I.M. Khrapova, A.V. Polonskii and N.N. Korneev, J. Organomet. Chem., 406 (1991) 139.
9. [8] W. Ziemkowska, S. Pasynkiewicz and E. Kalbarczyk, J. Organomet. Chem., 465 (1994) 93; L.A. Nekhaeva, G.N. Bondarenko, S.V. Rykov, A.I. Nekhaev, B.A. Krentsel, V.P. Mar'in, L.I. Vyshinskaya, I.M. Khrapova, A.V. Polonskii and N.N. Korneev, J. Organomet. Chem., 406 (1991) 139.
10. [9] G. Kurek, Dissertation, Universität zu Köln, 1994.
11. 27Al) = 148.6 ppm).
12. [11] See also P. Jutzi, Chem. Rev., 86 (1986) 983.
13. [12] H. Shapiro, E.G. Dewitt and J.E. Brown, US, Patent 2 987 534, 1961.
14. [13] A. Haaland and J. Weidlein, J. Organomet. Chem., 40 (1972) 29.
15. [14] D.A. Drew and A. Haaland, Acta Chem. Scand., 27 (1973) 3735.
16. [15] J. Stadelhofer, J. Weidlein, P. Fischer and A. Haaland, J. Organomet. Chem., 116 (1976) 55.
17. [16] B. Teclé, W.R. Corfield and J.P. Oliver, Inorg. Chem., 21 (1982) 458.
18. [17] J.K. Beattie and K.W. Nugent, Inorg. Chim. Acta, 198 (1992) 309.
19. [18] P. Fischer, J. Stadelhofer and J. Weidlein, J. Organomet. Chem., 116 (1976) 65.
20. 27Al NMR signals dynamic NMR studies were not useful.