A practical synthesis of ethynylferrocene from ferrocene carboxaldehyde: Structure of 1,4-diferrocenyl-1,3-butadiyne

Journal of Organometallic Chemistry

Volumn 513, Issue 1-2, 1996, Pages 71-76

  Rodriguez, José Gonzalo ^a   Oñate, Antonio ^a   Martin Villamil, Rosa M ^a   Fonseca, Isabel ^a  

^a NONE

Author keywords

Diynes; Ferrocenes; Synthesis; Wittig reaction; X ray crystal structure

Indexed keywords

EID: 0030567467     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/0022-328X(95)05943-J     Document Type: Article

References (28)

1. [1] I.R. Butler, in E.W. Abel (ed.), Organometallic Chemistry, Vol. 21, Royal Society of Chemistry, London, 1992, pp. 338-340.
2. [2] R.W. Wagner, P.A. Brown, T.E. Johnson and J.S. Lindsey, J. Chem. Soc. Chem. Commun. (1991) 1463.
3. [3] E.C. Constable, Angew Chem. Int. Ed. Engl., 30 (1991) 407.
4. [4] K.M. Chi, J.C. Calabrese, W.M. Reiff and J.S. Miller, Organometallics, 10 (1991) 668.
5. [5] C. Kollmar, M. Couty and O. Kahn, J. Am. Chem. Soc., 113 (1991) 7994.
6. [6] S.R. Marder, in D.W. Bruce and D. O'Hare (eds.), Inorganic Materials, Wiley, Chichester, 1992, p. 115 and references cited therein.
7. [7] (a) Z. Yuan, G. Stringer, I.R. Jobe, D. Kreller, K. Scott, L. Koch, N.J. Taylor and T.B. Marder, J. Organomet. Chem., 452 (1993) 115;
8. (b) K.L. Kott, D.A. Higgins, R.J. McMahon and R.C. Corn, J. Am. Chem. Soc., 115 (1993) 5342, and references cited therein.
9. [8] J.L. Oudar and D.S. Chemla, J. Chem. Phys., 66 (1977) 2664; B.F. Levine and C.C. Betea, J. Chem. Phys., 66 (1977) 1070.
10. [8] J.L. Oudar and D.S. Chemla, J. Chem. Phys., 66 (1977) 2664; B.F. Levine and C.C. Betea, J. Chem. Phys., 66 (1977) 1070.
11. [9] M.L.H. Green, S.R. Marder, M.E. Thompson, J.A. Bandy, D. Bloor, P.V. Kolinsky and R.J. Jones, Nature, 330 (1987) 360; J.C. Calabrese, L.-T. Cheng, J.C. Green, S.R. Marder and W. Tam, J. Am. Chem. Soc., 113 (1991) 7227.
12. [9] M.L.H. Green, S.R. Marder, M.E. Thompson, J.A. Bandy, D. Bloor, P.V. Kolinsky and R.J. Jones, Nature, 330 (1987) 360; J.C. Calabrese, L.-T. Cheng, J.C. Green, S.R. Marder and W. Tam, J. Am. Chem. Soc., 113 (1991) 7227.
13. [10] J.F. Nicoud and R.J. Twieg, in D.S. Chemia and J. Zyss (eds.), Nonlinear Optical Properties of Organic Molecules and Crystals, Academic Press, New York, 1987.
14. [11] K. Schlögl and H. Egger, Monatsh. Chem., 94 (1963) 376.
15. [12] J. March, Advanced Organic Chemistry, Wiley-Interscience, New York, 1992, 3rd edn., pp. 335-338.
16. [13] W.D.S. Motherwell and W. Clegg, PLUTO. A program for plotting crystal and molecular structures, 1978 (Cambridge University, UK).
17. [14] P. Seiler and J.D. Dunitz, Acta Crystallogr Sect. B, 38 (1982) 1741.
18. [15] S.L. Ingham, M.S. Khan, J. Lewis, N.J. Long, and P.R. Raithby, J. Organomet. Chem., 470 (1994) 153.
19. [16] J.G. Rodríguez et al., in preparation.
20. [17] A. Albert and F.H. Cano, CONTACTOS. A program for systematic study of aromatic rings interactions, 1990 (Institute Rocasolano, CSIC, Madrid).
21. [18] M. Rosenblum, N. Brown, J. Papemeir and M. Applelbaum, J. Organomet. Chem., 6 (1966) 173.
22. [19] A. Altomare, G. Cascarano, C. Giacovazzo and A. Guagliardi, Dip. Geomineralogico, University of Bari; M.C. Burla, G. Polidori, Dip. Scienze della Terra, University of Perugia; M. Camalli, 1st. Strutt. Chimica, CNR, Monterrotondo Stazione, Roma SIR92 (1992).
23. [19] A. Altomare, G. Cascarano, C. Giacovazzo and A. Guagliardi, Dip. Geomineralogico, University of Bari; M.C. Burla, G. Polidori, Dip. Scienze della Terra, University of Perugia; M. Camalli, 1st. Strutt. Chimica, CNR, Monterrotondo Stazione, Roma SIR92 (1992).
24. [19] A. Altomare, G. Cascarano, C. Giacovazzo and A. Guagliardi, Dip. Geomineralogico, University of Bari; M.C. Burla, G. Polidori, Dip. Scienze della Terra, University of Perugia; M. Camalli, 1st. Strutt. Chimica, CNR, Monterrotondo Stazione, Roma SIR92 (1992).
25. [20] J.M. Stewart, F.A. Kundell and J.C. Baldwin. The XRAY 80 System, 1976 (Computer Science Center, University of Maryland, College Park, Maryland).
26. [21] M. Martínez-Ripoll and F.H. Cano, PESOS. A computer program for the automatic treatment of weighting schemes, 1975 (Instituto Rocasolano, CSIC, Madrid).
27. [22] International Tables for X-ray Crystallography, Vol. 4, Kynoch, Birmingham, 1974.
28. [23] M. Nardelli, 1983 PARST, Comput. Chem., 7 (1983) 95.