NMR assignments and conformational studies of new C3-cyclotriveratrylenes with pendant thiol substituents

Magnetic Resonance in Chemistry

Volumn 34, Issue 1, 1996, Pages 24-32

  Bougault, Catherine ^a   Jordanov, Jeanne ^a   Bardet, Michel ^a  

^a CEA GRENOBLE   (France)

Author keywords

13C NMR; 1H NMR; C3 cyclotriveratrylenic trithiols; Conformational studies; Force field calculations; NMR; NOE quantitative measurements

Indexed keywords

CRYSTAL STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; X RAY ANALYSIS;

13C NMR; 1H NMR; C3-CYCLOTRIVERATRYLENIC TRITHIOL; CONFORMATIONAL STUDY; CYCLOTRIVERATRYLENES; FORCE FIELD CALCULATIONS; NMR ASSIGNMENT; NMR SPECTRUM; NOE QUANTITATIVE MEASUREMENT; QUANTITATIVE MEASUREMENT;

CONFORMATIONS;

EID: 0030552891     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1097-458X(199601)34:1<24::AID-OMR836>3.0.CO;2-7     Document Type: Article

References (17)

1. (a) J. P. Collman, X. Zhang, R. T. Hembre and J. I. Brauman, J. Am. Chem. Soc. 112, 5326 (1990); (b) L. C. Chiang, K. Konishi, T. Aida and S. Inoue, J. Chem. Soc., Chem. Commun. 254 (1992), and references cited therein.
2. (a) J. P. Collman, X. Zhang, R. T. Hembre and J. I. Brauman, J. Am. Chem. Soc. 112, 5326 (1990); (b) L. C. Chiang, K. Konishi, T. Aida and S. Inoue, J. Chem. Soc., Chem. Commun. 254 (1992), and references cited therein.
3. (a) S. Ciurli, M. Carrié, J. A. Weigel, M. J. Carney, T. D. P. Stack, G. C. Papaefthymiou and R. H. Holm. J. Am. Chem. Soc. 112, 2654 (1990); (b) M. A. Whitener, G. Peng and R. H. Holm, Inorg. Chem. 30, 2411 (1991).
4. (a) S. Ciurli, M. Carrié, J. A. Weigel, M. J. Carney, T. D. P. Stack, G. C. Papaefthymiou and R. H. Holm. J. Am. Chem. Soc. 112, 2654 (1990); (b) M. A. Whitener, G. Peng and R. H. Holm, Inorg. Chem. 30, 2411 (1991).
5. T. B. Karpishin, T. D. P. Stack and K. N. Raymond, J. Am. Chem. Soc. 115, 182 (1993).
6. C. Bougault, M. Bardet, J. Laugier, J. Jordanov, J. P. Dutasta and A. Collet, Supramol. Chem. 4, 139 (1994).
7. D. Neuhaus and M. Williamson, The Nuclear Overhauser Effect in Structural and Conformational Analysis. VCH, New York (1989).
8. G. Bodenhausen and R. R. Ernst, J. Am. Chem. Soc. 104, 1304 (1982).
9. S. Macura, B. T. Farmer and L. R. Brown, J. Magn. Reson. 70, 493 (1986).
10. G. Esposito and A. Pastore, J. Magn. Reson. 76, 331 (1988).
11. M. Reggelin, H. Hoffmann, M. Köck and D. F. Mierke, J. Am. Chem. Soc. 114, 3272 (1992).
12. S. Cerrini, E. Giglio, F. Mazza and N. V. Pavel, Acta Crystallogr., Sect. B 35, 2605 (1979).
13. (a) A. Collet, J. Gabard, J. Jacques, M. Cesario, J. Guilhem and C. Pascard, J. Chem. Soc., Perkin Trans. 1 1630 (1981); (b) J. A. Hyatt, E. N. Duessler, D. Y. Curtin and I. C. Paul, J. Org. Chem. 45, 5074 (1980).
14. (a) A. Collet, J. Gabard, J. Jacques, M. Cesario, J. Guilhem and C. Pascard, J. Chem. Soc., Perkin Trans. 1 1630 (1981); (b) J. A. Hyatt, E. N. Duessler, D. Y. Curtin and I. C. Paul, J. Org. Chem. 45, 5074 (1980).
15. D. F. Ewing, Org. Magn. Reson. 2, 499 (1979).
16. A. Collet, in Inclusion Compounds, edited by J. L. Atwood, Vol. II, Chapt. 4. Academic Press, London (1984).
17. J. Canceill, A. Collet, J. Gabard, G. Gotarelli and P. Spada, J. Am. Chem. Soc. 107, 1299 (1985).