6,6-bis(carboxy-2-oxabutyl)-4,8-dioxaundecane-1,11-dicarboxylic acid

Organic Preparations and Procedures International

Volumn 28, Issue 2, 1996, Pages 242-244

  Newkome, George R ^a   Weis, Claus D ^a  

^a UNIVERSITY OF SOUTH FLORIDA   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

DICARBOXYLIC ACID;

EID: 0030552439     PISSN: 00304948     EISSN: 19455453     Source Type: Journal    
DOI: 10.1080/00304949609356531     Document Type: Article

References (15)

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3. G. R. Newkome, S. Arai, F. R. Fronczek, C. N. Moorefield, X. Lin and C. D. Weis, J. Org. Chem., 58, 898 (1993).
4. H. A. Bruson and T. W. Riener, J. Am. Chem. Soc., 65, 23 (1943).
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6. H. A. Bruson (The Resinous Products and Chemical Corp.), US Patent, 2, 437, 905 (1941); Chem. Abstr., 42, 4195 (1942).
7. H. Meerwein in “Methoden der Organische Chemie (Houben-Weyl)”, Vol. VI/3, p. 23
8. E. Mueller, Ed., Georg Thieme Verlag, Stuttgart, 1965.
9. G. R. Newkome and X. Lin, Macromolecules, 24, 1443 (1991).
10. C. J. Schmidle and R. C. Mansfield, bid. Eng. Chem., 44, 1338 (1952).
11. I. G. Farben, Germ. Patent, 731, 708 (1940); Chem. Abstr., 38, 5555 (1944).
12. G. R. Newkome, C. D. Weis, X. Lin and F. R. Fronczek, Acta Cryst., C49, 998 (1993).
13. G. R. Newkome, C. N. Moorefield and K. J. Theriot, J. Org. Chem., 53, 5552 (1988).
14. F. Sorm and G. Beranek, Collect. Czech. Chem. Commun., 19, 298 (1954).
15. The reaction may became slightly exothermic; the temperature, however, should not exceed 8085°, since higher temperatures enhanced the formation of oily by-products which hampered considerably crystallization of the acid.