Electrochemical deacetylation of 1,3-dicarbonyl compounds

Chemistry Letters

Volumn , Issue 2, 1996, Pages 143-144

  Fujimoto, Kazuo ^b   Maekawa, Hirofumi ^a   Matsubara, Yoshiharu ^b   Nishiguchi, Ikuzo ^a  

^a OSAKA MUNICIPAL TECHNICAL RESEARCH INSTITUTE   (Japan)

^b KINKI UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0030541314     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1996.143     Document Type: Article

References (13)

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4. -2). After 4F/mol electricity was passed, the product was isolated by distillation.
5. Almost recovery of methyl benzylacetoacetates (1a) on treatment of 1a with EtOH/EtONa denied the possibility of base-catalyzed deacetylation.
6. T. Shono, Y. Matsumura, H. Hamaguchi, T. Imanishi, and K. Yoshida, Bull. Chem. Soc. Jpn., 51, 2179 (1978).
7. Yields were determined by gas chromatography analysis.
8. M. M. Baizer, T. Nonaka, K. Park, Y. Saito, and K. Nobe, J. Appl. Electrochem., 14, 197 (1984).
9. H . Maekawa, K. Nakano, T. Hirashima, and I. Nishiguchi, Chem. Lett., 1991, 1661.
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12. b) W. L. Meyer, A. P. Lobo, and E. T. Marquis, J. Org. Chem., 30, 181 (1965).
13. N. T. Albertson, J. Am. Chem. Soc., 70, 669 (1948).