Combined DEPT 1D and INEPT DQF COSY 2D experiments in 29Si NMR spectroscopy of alkoxysilane polymers: 1 - New polarization transfer NMR methods

Magnetic Resonance in Chemistry

Volumn 34, Issue 2, 1996, Pages 100-108

  Lux, P ^a,b   Brunet, F ^a   Virlet, J ^a   Cabane, B ^a  

^a CEA SACLAY   (France)

^b Bruker Spectrospin   (France)

Author keywords

29Si NMR; coherence transfer optimization; DEPT; dimethyldiethoxysilane; editing method; NMR; polymers

Indexed keywords

POLARIZATION;

29SI NMR; ALKOXYSILANES; COHERENCE TRANSFER; COHERENCE TRANSFER OPTIMIZATION; DEPT; DIMETHYLDIETHOXYSILANE; EDITING METHOD; NMR-SPECTROSCOPY; OPTIMISATIONS; POLARIZATION-TRANSFER;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

EID: 0030535725     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1097-458X(199602)34:2<100::AID-OMR844>3.0.CO;2-4     Document Type: Article

References (41)

1. C. J. Brinker and G. W. Scherer, Sol-Gel Science. Academic Press, New York (1990).
2. R. K. Iler, The Chemistry of Silica. Wiley, New York (1979).
3. Z. Grubisic-Gallot, F. Schosseler, P. Lixon and B. Cabane, Macromolecules 25, 3733 (1992).
4. M. Dubois and B. Cabane, Macromolecules 22, 2526 (1989).
5. B. Cabane, M. Dubois, F. Lefaucheux and M. C. Robert, J. Non-Cryst. Solids 119, 121 (1990).
6. G. Engelhardt and D. Michel, High Resolution Solid State NMR of Silicates and Zeolites. Wiley, New York (1987).
7. R. K. Harris, C. T. G. Knight and W. E. Hull, J. Am Chem. Soc. 103, 1577 (1981).
8. R. K. Harris, N. J. O'Connor, E. H. Curzon and O. W. Howarth, J. Magn. Reson. 57, 115 (1984).
9. Th. Blinka, B. J. Helmer and R. West, Adv. Organomet. Chem. 23, 193 (1984).
10. G. A. Morris and R. Freeman, J. Am. Chem. Soc. 101, 760 (1979).
11. D. M. Doddrell, D. T. Pegg and M. R. Bendall, J. Magn. Reson. 48, 323 (1982).
12. D. T. Pegg, D. M. Doddrell and M. R. Bendall, J. Chem. Phys. 77, 2745 (1982).
13. O. W. Sorensen, Prog. Nucl. Magn. Reson. Spectrosc. 21, 503 (1989).
14. J. Schraml, Collect. Czech. Chem. Commun. 48, 3402 (1983).
15. F. Bruney, B. Cabane, M. Dubois and B. Perly, J. Phys. Chem. 163, 945 (1991).
16. F. Bruney and B. Cabane, J. Non-Cryst. Solids 163, 211 (1993).
17. P. Lux, F. Brunet, H. Desvaux and J. Virlet, Magn. Reson. Chem. 31, 623 (1993).
18. M. Rance, G. Wagner, O. W. Sorensen, K. Wuthrich and R. R. Ernst, J. Magn. Reson. 59, 250 (1984).
19. A. Bax and R. Freeman, J. Magn. Reson. 44, 542 (1981).
20. R. R. Ernst, G. Bodenhausen and A. Wokaun, Principles of Nuclear Magnetic Resonance in One and Two Dimensions. Clarendon Press, Oxford (1987).
21. O. W. Sorensen, G. W. Eich, M. H. Levitt, G. Bodenhausen and R. R. Ernst, Prog. Nucl. Magn. Reson. Spectrosc. 16, 163 (1983).
22. H. Kessler, M. Gehrke and C. Giesinger, Angew. Chem., Int. Ed. Engl. 27, 490 (1988).
23. H. Kessler, C. Griesinger, J. Zarbock and H. R. Loosli, J. Magn. Reson. 57, 331 (1984).
24. R. Freeman and G. A. Morris, J. Chem. Soc., Chem. Commun., 684 (1978).
25. A. Bax and G. Morris, J. Magn. Reson. 42, 501 (1981).
26. V. V. Krishnamurthy and J. E. Casida, Magn. Reson. Chem. 26, 362 (1988).
27. V. V. Krishnamurthy and J. E. Casida, Magn. Reson. Chem. 26, 367 (1988).
28. G. E. Martin and A. S. Zektzer, Two-Dimensional NMR Methods for Establishing Molecular Connectivity: a Chemist's Guide to Experiment Selection, Performance and Interpretation, VCH, New York (1988).
29. M. Perpick-Dumont, R. G. Enriquez, S. McLean, F. V. Puzzuoli and W. F. Reynolds, J. Magn. Reson. 75, 414 (1987).
30. W. F. Reynolds, S. McLean, M. Perpick-Dumont and R. G. Enriquez, Magn. Reson. Chem. 27, 162 (1984).
31. R. H. Glaser, G. L. Wilkes and C. E. Bronnimann, J. Non-Cryst. Solids 113, 73 (1989).
32. R. K. Harris and B. J. Kimber, J. Magn. Reson. 17, 174 (1975).
33. R. K. Harris and B. J. Kimber, Org. Magn. Reson. 7, 460 (1975).
34. E. Liepins, I. Zichane and E. Lukevics, J. Organomet. Chem. 306, 167 (1986).
35. F. Babonneau, K. Thorne and J. D. Mackenzie, Chem. Mater. 1, 554 (1989).
36. Y. Sugahara, S. Okada, K. Kuroda and C. Kato, J. Non-Cryst. Solids 139, 25 (1992).
37. J. C. Pouxviel, J. P. Boilot, J. C. Beloeil and J. Y. Lallemand, J. Non-Cryst. Solids 94, 374 (1987).
38. L. W. Kelts, N. J. Effinder and S. M. Mepolder, J. Non-Cryst. Solids 83, 353 (1986).
39. I. Artaki, T. W. Zerda and J. Jonas, J. Phys. Chem. 89, 4399 (1985).
40. J. J. Van Beek, D. Seykens, J. B. H. Jansen and R. D. Schuiling, J. Non-Cryst. Solids 134, 14 (1991).
41. M. J. Van Bommel, T. N. M. Bernards and A. H. Boonstra, J. Non-Cryst. Solids 128, 231 (1991).