Further NMR investigation and conformational analysis of an acylated flavonol glucorhamnoside

Magnetic Resonance in Chemistry

Volumn 34, Issue 4, 1996, Pages 249-254

  Gao, Jinhai ^a   Shi, Genbin ^a   Song, Guoqiang ^a   Shao, Yu ^a   Zhou, Bingnan ^a  

^a SHANGHAI INSTITUTE OF MATERIA MEDICA   (China)

Author keywords

2D NMR; Acylated flavonol glucorhamnoside; Conformational analysis; Hydrogen bond; Molecular dynamics

Indexed keywords

ACYLATION; CONFORMATIONS; FLAVONOIDS; HYDROGEN BONDS; HYDROPHOBICITY; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

2-D NMR; ACYLATED FLAVONOL GLUCORHAMNOSIDE; CONFORMATIONAL ANALYSIS; DYNAMICS SIMULATION; FOLDED CONFORMATION; KAEMPFEROL; NMR DATA; NMR TECHNIQUES; PERIODIC BOUNDARY CONDITIONS; RESONANCE ASSIGNMENTS;

MOLECULAR DYNAMICS;

EID: 0030531538     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1097-458X(199604)34:4<249::AID-OMR877>3.0.CO;2-O     Document Type: Article

References (25)

1. S. S. Kang, J. S. Kim, W.-J. Kwak and K.-H. Kim. Kor. J. Pharmacogn. 21, 111 (1990).
2. S. S. Kang, J. S. Kim, W.-J. Kwak and K.-H. Kim, Arch. Pharm. Res. 13, 207 (1990).
3. C. Naser, M. Haag-Berruier, A. Lobstrin-Guth and R. Anton, Phytochemistry 25, 770 (1986).
4. T. Goto and T. Kondo, Angew. Chem., Int. Ed. Engl. 30, 17 (1991).
5. T. Goto, T. Kondo, H. Tamura and K. Kawahori, Tetrahedron Lett. 24, 2181 (1983).
6. M. Williams and G. Hrazdina, J. Food Sci. 44, 66 (1979)
7. T. Goto, H. Tamura, T. Kawai, T. Hoshino, N. Harada and T. Kondo, Ann. N.Y. Acad. Sci. 471, 155 (1986).
8. U. Piantini, O. W. Sørensen and R. R. Ernst, J. Am. Chem. Soc. 104, 6800 (1982).
9. J. Jeener, B. H. Meier, P. Bachmann and R. R. Ernst, J. Chem. Phys. 71, 4546 (1979).
10. A. Bax and G. A. Morris, J. Magn. Reson. 42, 501 (1981).
11. A. Bax and D. G. Davis, J. Magn. Reson. 63, 207 (1985).
12. A. Bax and M. F. Summers, J. Am. Chem. Soc. 108, 209 (1986).
13. D. Neuhaus and M. Williamson, The NOE Effect in Structural and Conformational Analysis. VCH, Weinheim (1989).
14. D. F. Mierke and H. Kessler, J. Am. Chem. Soc. 113, 9466 (1991).
15. W. F. van Gunsteren and H. J. C. Berendsen, Mol. Phys. 34, 1311 (1977).
16. H. J. C. Berendsen, J. P. M. Postma, W. F. van Gunsteren, A. DiNola and J. R. Haak, J. Chem. Phys. 81, 3684 (1984).
17. C. A. G. Haasnoot, F. M. de Leeuw and C. Altona, Tetrahedron 36, 2783 (1980).
18. R. J. Abraham, E. J. Chambers and W. A. Thomas, Carbohydr. Res. 226, c1-c5 (1992).
19. Y. Nishida, H. Hori, Y. Ohrui and H. Meguro, J. Carbohydr. Chem. 7, 239 (1988).
20. Y. Nishida, Y. Ohrui and H. Meguro, Tetrahedron Lett. 125, 1575 (1984).
21. M. St-Jacques, P. R. Sundararajan, K. J. Taylor and R. H. Marchessault, J. Am. Chem. Soc. 98, 4386 (1976).
22. L. Poppe, C.-W. von der Lieth and J. Dabrowski, J. Am. Chem. Soc. 112, 7762 (1990).
23. D. Acquotti, L. Poppe, J. Dabrowski, C.-W. von der Lieth, S. Sonnino and G. Tettamanti, J. Am. Chem. Soc. 112, 7772 (1990).
24. B. Adams and L. Lerner, J. Am. Chem. Soc. 114, 4827 (1992).
25. R. R. Fraser, M. Kaufman, P. Morand and G. Govil, Can. J. Chem. 47, 403 (1969).