Synthesis, structure, and electrochemistry of a dodecanuclear chromium cluster complex [Cr12S16(PEt3)10]

Chemistry Letters

Volumn , Issue 7, 1996, Pages 555-556

  Kamiguchi, Satoshi ^a   Imoto, Hideo ^a   Saito, Taro ^a  

^a UNIVERSITY OF TOKYO   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0030521534     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1996.555     Document Type: Article

References (13)

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2. H. Nohl, W. Klose, and O. K. Andersen, in "Superconductivity in Ternary Compounds I," ed by Ø. Fischer and M. B. Maple, Springer, Berlin (1982), pp. 165-221.
3. B. Hessen, T. Siegrist, T. Palstra, S. M. Tanzler, and M. L. Steigerwald, Inorg. Chem., 32, 5165 (1993).
4. K. Tsuge, H. Imoto, and T. Saito, Bull. Chem. Soc. Jpn., 69, 627 (1996).
5. 0|); 6° < 2θ < 55°). The intensity data were collected by a Rigaku AFC-7R diffractometer with Mo Kα radiation at 207 K. In the crystal structure analyses, the positions of the chromium atoms were determined by direct methods (SHELXS86),11 and other non-hydrogen atoms were located on Fourier maps (SHELXS76). 12 The full-matrix refinements were performed with programs SHELXS76 and ANYBLK. 13 Hydrogen atoms were not included in the refinements.
6. F. Cecconi, C. A. Ghilardi, S. Midollini, and A. Orlandini, Inorg. Chim. Acta, 214, 13 (1993).
7. C. Mealli and A. Orlandini, Gazz. Chim. Ital., 125, 271 (1995).
8. L. Pauling, "The Nature of the Chemical Bond," Cornell University Press, Ithaca, New York (1960), p. 233.
9. J. A. Baumann, D. J. Salmon, S. T. Wilson, and T. J. Meyer, Inorg. Chem., 18, 2472 (1979).
10. T. Saito and H. Imoto, Bull. Chem. Soc. Jpn., to be published.
11. G. M. Scheldrick, "SHELXS86, a program for crystal structure determination," University of Cambridge, U.K., (1986).
12. G. M. Scheldrick, "SHELXS76, a program for crystal structure determination," University of Cambridge, U.K., (1976).
13. H. Imoto, S. Hayakawa, N. Morita, and T. Saito, Inorg. Chem., 29, 2007 (1990).