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85033009546
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note
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All PEG-supported products were isolated by precipitation from tert-butyl methyl ether as described [3], Yields were calculated based on mass balances and do not necessarily reflect the purity.
-
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15
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0001325832
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18
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85033033320
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1H NMR spectrometer
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1H NMR spectrometer.
-
-
-
-
19
-
-
85033007378
-
-
note
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2; 2. NaOMe/ MeOH).
-
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20
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0001648945
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85033017144
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note
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2).
-
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-
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22
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85033020484
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-
note
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2O/MeOH (1/1).
-
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24
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0024816685
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25
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-
85033026793
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-
note
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2 (α:β = 1.2:1).
-
-
-
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26
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33845278486
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K. Jansson, S. Ahlfors, T. Freid, J. Kihlberg, G. Magnusson, J. Org. Chem. 1988, 53, 5629-5647; T. Fukuyama, A. A. Laird, L. M. Hotchkiss, Tetrahedron Lett. 1985, 26, 6291-6292.
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46549104605
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