-
1
-
-
0000964106
-
-
H.-D. Martin, B. Mayer, Angew. Chem. 1983, 95, 281; Angew. Chem. Int. Ed. Engl. 1983, 22, 283; J. J. Wolff, ibid. 1995, 107, 2409 and 1995, 34, 2225, and references therein.
-
(1983)
Angew. Chem.
, vol.95
, pp. 281
-
-
Martin, H.-D.1
Mayer, B.2
-
2
-
-
0343658572
-
-
H.-D. Martin, B. Mayer, Angew. Chem. 1983, 95, 281; Angew. Chem. Int. Ed. Engl. 1983, 22, 283; J. J. Wolff, ibid. 1995, 107, 2409 and 1995, 34, 2225, and references therein.
-
(1983)
Angew. Chem. Int. Ed. Engl.
, vol.22
, pp. 283
-
-
-
3
-
-
85033018033
-
-
H.-D. Martin, B. Mayer, Angew. Chem. 1983, 95, 281; Angew. Chem. Int. Ed. Engl. 1983, 22, 283; J. J. Wolff, ibid. 1995, 107, 2409 and 1995, 34, 2225, and references therein.
-
(1995)
Angew. Chem. Int. Ed. Engl.
, vol.107
, pp. 2409
-
-
Wolff, J.J.1
-
4
-
-
33748242056
-
-
and references therein
-
H.-D. Martin, B. Mayer, Angew. Chem. 1983, 95, 281; Angew. Chem. Int. Ed. Engl. 1983, 22, 283; J. J. Wolff, ibid. 1995, 107, 2409 and 1995, 34, 2225, and references therein.
-
(1995)
Angew. Chem. Int. Ed. Engl.
, vol.34
, pp. 2225
-
-
-
5
-
-
0000148462
-
-
and references therein
-
H. Prinzbach, G. Gescheidt, H.-D. Martin, R. Herges, J. Heinze, G. K. Surya Prakash, G. A. Olah, Pure Appl. Chem. 1995, 67, 673, and references therein.
-
(1995)
Pure Appl. Chem.
, vol.67
, pp. 673
-
-
Prinzbach, H.1
Gescheidt, G.2
Martin, H.-D.3
Herges, R.4
Heinze, J.5
Surya Prakash, G.K.6
Olah, G.A.7
-
6
-
-
0030600187
-
-
a) T. Mathew, M. Keller, D. Hunkler, H. Prinzbach, Tetrahedron Lett. 1996, 37, 4491;
-
(1996)
Tetrahedron Lett.
, vol.37
, pp. 4491
-
-
Mathew, T.1
Keller, M.2
Hunkler, D.3
Prinzbach, H.4
-
7
-
-
0001130422
-
-
b) H. Prinzbach, G. Sedelmeier, C. Krüger, R. Goddard, H.-D. Martin, R. Gleiter, Angew. Chem. 1978, 90, 297; Angew. Chem. Int. Ed. Engl. 1978, 17, 271; G. Sedelmeier. W.-D. Fessner, C. Grund, P. R. Spurr, H. Fritz, H. Prinzbach. Tetrahedron Lett. 1986, 27, 1277.
-
(1978)
Angew. Chem.
, vol.90
, pp. 297
-
-
Prinzbach, H.1
Sedelmeier, G.2
Krüger, C.3
Goddard, R.4
Martin, H.-D.5
Gleiter, R.6
-
8
-
-
84985609821
-
-
b) H. Prinzbach, G. Sedelmeier, C. Krüger, R. Goddard, H.-D. Martin, R. Gleiter, Angew. Chem. 1978, 90, 297; Angew. Chem. Int. Ed. Engl. 1978, 17, 271; G. Sedelmeier. W.-D. Fessner, C. Grund, P. R. Spurr, H. Fritz, H. Prinzbach. Tetrahedron Lett. 1986, 27, 1277.
-
(1978)
Angew. Chem. Int. Ed. Engl.
, vol.17
, pp. 271
-
-
-
9
-
-
0001078935
-
-
b) H. Prinzbach, G. Sedelmeier, C. Krüger, R. Goddard, H.-D. Martin, R. Gleiter, Angew. Chem. 1978, 90, 297; Angew. Chem. Int. Ed. Engl. 1978, 17, 271; G. Sedelmeier. W.-D. Fessner, C. Grund, P. R. Spurr, H. Fritz, H. Prinzbach. Tetrahedron Lett. 1986, 27, 1277.
-
(1986)
Tetrahedron Lett.
, vol.27
, pp. 1277
-
-
Sedelmeier, G.1
Fessner, W.-D.2
Grund, C.3
Spurr, P.R.4
Fritz, H.5
Prinzbach, H.6
-
10
-
-
0343222913
-
-
W. Berning, S. Hünig, Angew. Chem. 1977, 89, 825; Angew. Chem. Int. Ed. Engl. 1977, 16, 777; S. Hünig, P. Kraft, J. Prukt. Chem. 1990, 332, 133; S. Hünig, P. Kraft, F.-G. Klärner, U. Artschwager-Perl, K. Peters, H.-G. von Schnering, Liebigs Ann. 1995, 351, and references therein.
-
(1977)
Angew. Chem.
, vol.89
, pp. 825
-
-
Berning, W.1
Hünig, S.2
-
11
-
-
84980185241
-
-
W. Berning, S. Hünig, Angew. Chem. 1977, 89, 825; Angew. Chem. Int. Ed. Engl. 1977, 16, 777; S. Hünig, P. Kraft, J. Prukt. Chem. 1990, 332, 133; S. Hünig, P. Kraft, F.-G. Klärner, U. Artschwager-Perl, K. Peters, H.-G. von Schnering, Liebigs Ann. 1995, 351, and references therein.
-
(1977)
Angew. Chem. Int. Ed. Engl.
, vol.16
, pp. 777
-
-
-
12
-
-
0004723560
-
-
W. Berning, S. Hünig, Angew. Chem. 1977, 89, 825; Angew. Chem. Int. Ed. Engl. 1977, 16, 777; S. Hünig, P. Kraft, J. Prukt. Chem. 1990, 332, 133; S. Hünig, P. Kraft, F.-G. Klärner, U. Artschwager-Perl, K. Peters, H.-G. von Schnering, Liebigs Ann. 1995, 351, and references therein.
-
(1990)
J. Prukt. Chem.
, vol.332
, pp. 133
-
-
Hünig, S.1
Kraft, P.2
-
13
-
-
84988091833
-
-
and references therein
-
W. Berning, S. Hünig, Angew. Chem. 1977, 89, 825; Angew. Chem. Int. Ed. Engl. 1977, 16, 777; S. Hünig, P. Kraft, J. Prukt. Chem. 1990, 332, 133; S. Hünig, P. Kraft, F.-G. Klärner, U. Artschwager-Perl, K. Peters, H.-G. von Schnering, Liebigs Ann. 1995, 351, and references therein.
-
(1995)
Liebigs Ann.
, pp. 351
-
-
Hünig, S.1
Kraft, P.2
Klärner, F.-G.3
Artschwager-Perl, U.4
Peters, K.5
Von Schnering, H.-G.6
-
14
-
-
0142009122
-
-
and references therein
-
S. F. Nelson, M. R. Willi, J. Org. Chem. 1984, 49, 1, and references therein: J. Kettenring, D. Ginsburg, Tetrahedron 1984, 40, 5269; G. Fischer, D. Hunkler, H. Prinzbach, G. Rihs, H. Fritz, Tetrahedron Lett. 1984, 25, 2459; W. Marterer, H. Prinzbach, G. Rihs, J. Wirz, J. Lecoultre, E. Heilbronner, Helv. Chim. Acta 1988, 71, 1937; for "orthogonal" azo/enes see: K.-H. Lehr, R. Hildebrand, H. Fritz, L. Knothe, C. Krüger, H. Prinzbach, Chem. Ber. 1982, 115, 1875.
-
(1984)
J. Org. Chem.
, vol.49
, pp. 1
-
-
Nelson, S.F.1
Willi, M.R.2
-
15
-
-
0342353379
-
-
S. F. Nelson, M. R. Willi, J. Org. Chem. 1984, 49, 1, and references therein: J. Kettenring, D. Ginsburg, Tetrahedron 1984, 40, 5269; G. Fischer, D. Hunkler, H. Prinzbach, G. Rihs, H. Fritz, Tetrahedron Lett. 1984, 25, 2459; W. Marterer, H. Prinzbach, G. Rihs, J. Wirz, J. Lecoultre, E. Heilbronner, Helv. Chim. Acta 1988, 71, 1937; for "orthogonal" azo/enes see: K.-H. Lehr, R. Hildebrand, H. Fritz, L. Knothe, C. Krüger, H. Prinzbach, Chem. Ber. 1982, 115, 1875.
-
(1984)
Tetrahedron
, vol.40
, pp. 5269
-
-
Kettenring, J.1
Ginsburg, D.2
-
16
-
-
0010687774
-
-
S. F. Nelson, M. R. Willi, J. Org. Chem. 1984, 49, 1, and references therein: J. Kettenring, D. Ginsburg, Tetrahedron 1984, 40, 5269; G. Fischer, D. Hunkler, H. Prinzbach, G. Rihs, H. Fritz, Tetrahedron Lett. 1984, 25, 2459; W. Marterer, H. Prinzbach, G. Rihs, J. Wirz, J. Lecoultre, E. Heilbronner, Helv. Chim. Acta 1988, 71, 1937; for "orthogonal" azo/enes see: K.-H. Lehr, R. Hildebrand, H. Fritz, L. Knothe, C. Krüger, H. Prinzbach, Chem. Ber. 1982, 115, 1875.
-
(1984)
Tetrahedron Lett.
, vol.25
, pp. 2459
-
-
Fischer, G.1
Hunkler, D.2
Prinzbach, H.3
Rihs, G.4
Fritz, H.5
-
17
-
-
0001608264
-
-
S. F. Nelson, M. R. Willi, J. Org. Chem. 1984, 49, 1, and references therein: J. Kettenring, D. Ginsburg, Tetrahedron 1984, 40, 5269; G. Fischer, D. Hunkler, H. Prinzbach, G. Rihs, H. Fritz, Tetrahedron Lett. 1984, 25, 2459; W. Marterer, H. Prinzbach, G. Rihs, J. Wirz, J. Lecoultre, E. Heilbronner, Helv. Chim. Acta 1988, 71, 1937; for "orthogonal" azo/enes see: K.-H. Lehr, R. Hildebrand, H. Fritz, L. Knothe, C. Krüger, H. Prinzbach, Chem. Ber. 1982, 115, 1875.
-
(1988)
Helv. Chim. Acta
, vol.71
, pp. 1937
-
-
Marterer, W.1
Prinzbach, H.2
Rihs, G.3
Wirz, J.4
Lecoultre, J.5
Heilbronner, E.6
-
18
-
-
0006989131
-
-
S. F. Nelson, M. R. Willi, J. Org. Chem. 1984, 49, 1, and references therein: J. Kettenring, D. Ginsburg, Tetrahedron 1984, 40, 5269; G. Fischer, D. Hunkler, H. Prinzbach, G. Rihs, H. Fritz, Tetrahedron Lett. 1984, 25, 2459; W. Marterer, H. Prinzbach, G. Rihs, J. Wirz, J. Lecoultre, E. Heilbronner, Helv. Chim. Acta 1988, 71, 1937; for "orthogonal" azo/enes see: K.-H. Lehr, R. Hildebrand, H. Fritz, L. Knothe, C. Krüger, H. Prinzbach, Chem. Ber. 1982, 115, 1875.
-
(1982)
Chem. Ber.
, vol.115
, pp. 1875
-
-
Lehr, K.-H.1
Hildebrand, R.2
Fritz, H.3
Knothe, L.4
Krüger, C.5
Prinzbach, H.6
-
19
-
-
0013485689
-
-
L. A. Paquette, R. V. C. Carr, P. Charumilind, J. F. Blount, J. Org. Chem. 1980, 45, 4922; K. Beck, S. Hünig, Chem. Ber. 1987, 120, 477; B. Albert, W. Berning, C. Burschka, S. Hünig, F. Prokschy, ibid. 1984, 117, 1465.
-
(1980)
J. Org. Chem.
, vol.45
, pp. 4922
-
-
Paquette, L.A.1
Carr, R.V.C.2
Charumilind, P.3
Blount, J.F.4
-
20
-
-
84984177338
-
-
L. A. Paquette, R. V. C. Carr, P. Charumilind, J. F. Blount, J. Org. Chem. 1980, 45, 4922; K. Beck, S. Hünig, Chem. Ber. 1987, 120, 477; B. Albert, W. Berning, C. Burschka, S. Hünig, F. Prokschy, ibid. 1984, 117, 1465.
-
(1987)
Chem. Ber.
, vol.120
, pp. 477
-
-
Beck, K.1
Hünig, S.2
-
21
-
-
84984229619
-
-
L. A. Paquette, R. V. C. Carr, P. Charumilind, J. F. Blount, J. Org. Chem. 1980, 45, 4922; K. Beck, S. Hünig, Chem. Ber. 1987, 120, 477; B. Albert, W. Berning, C. Burschka, S. Hünig, F. Prokschy, ibid. 1984, 117, 1465.
-
(1984)
Chem. Ber.
, vol.117
, pp. 1465
-
-
Albert, B.1
Berning, W.2
Burschka, C.3
Hünig, S.4
Prokschy, F.5
-
22
-
-
0342308643
-
-
G. Fischer, E. Beckmann, H. Prinzbach, G. Rihs, J. Wirz, Tetrahedron Lett. 1986, 27, 1273.
-
(1986)
Tetrahedron Lett.
, vol.27
, pp. 1273
-
-
Fischer, G.1
Beckmann, E.2
Prinzbach, H.3
Rihs, G.4
Wirz, J.5
-
23
-
-
15744377334
-
-
K. Beck, S. Hünig, Angew. Chem. 1986, 98, 193; Angew. Chem. Int. Ed. Engl. 1986, 25, 187.
-
(1986)
Angew. Chem.
, vol.98
, pp. 193
-
-
Beck, K.1
Hünig, S.2
-
24
-
-
84985557293
-
-
K. Beck, S. Hünig, Angew. Chem. 1986, 98, 193; Angew. Chem. Int. Ed. Engl. 1986, 25, 187.
-
(1986)
Angew. Chem. Int. Ed. Engl.
, vol.25
, pp. 187
-
-
-
25
-
-
0001289274
-
-
H. Prinzbach, G. Fischer, G. Rihs, G. Sedelmeier, E. Heilbronner, Z. Yang, Tetrahedron Lett. 1982, 22, 1251; E. Beckmann, N. Bahr, H. Prinzbach, ibid. 1990, 31, 1125; N. Bahr, E. Beckmann, K. Mathauer, D. Hunkler, M. Keller, H. Prinzbach, H. Vahrenkamp, Chem. Ber. 1993, 126, 429.
-
(1982)
Tetrahedron Lett.
, vol.22
, pp. 1251
-
-
Prinzbach, H.1
Fischer, G.2
Rihs, G.3
Sedelmeier, G.4
Heilbronner, E.5
Yang, Z.6
-
26
-
-
0025176520
-
-
H. Prinzbach, G. Fischer, G. Rihs, G. Sedelmeier, E. Heilbronner, Z. Yang, Tetrahedron Lett. 1982, 22, 1251; E. Beckmann, N. Bahr, H. Prinzbach, ibid. 1990, 31, 1125; N. Bahr, E. Beckmann, K. Mathauer, D. Hunkler, M. Keller, H. Prinzbach, H. Vahrenkamp, Chem. Ber. 1993, 126, 429.
-
(1990)
Tetrahedron Lett.
, vol.31
, pp. 1125
-
-
Beckmann, E.1
Bahr, N.2
Prinzbach, H.3
-
27
-
-
0000859155
-
-
H. Prinzbach, G. Fischer, G. Rihs, G. Sedelmeier, E. Heilbronner, Z. Yang, Tetrahedron Lett. 1982, 22, 1251; E. Beckmann, N. Bahr, H. Prinzbach, ibid. 1990, 31, 1125; N. Bahr, E. Beckmann, K. Mathauer, D. Hunkler, M. Keller, H. Prinzbach, H. Vahrenkamp, Chem. Ber. 1993, 126, 429.
-
(1993)
Chem. Ber.
, vol.126
, pp. 429
-
-
Bahr, N.1
Beckmann, E.2
Mathauer, K.3
Hunkler, D.4
Keller, M.5
Prinzbach, H.6
Vahrenkamp, H.7
-
28
-
-
0242521029
-
-
J. M. Mellor, N. M. Smith, J. Chem. Res. Synop. 1985, 60; J. M. Mellor, R. Pathirana, N. M. Smith, J. Chem. Soc. Perkin Trans. 1 1988, 2501.
-
(1985)
J. Chem. Res. Synop.
, pp. 60
-
-
Mellor, J.M.1
Smith, N.M.2
-
29
-
-
37049072949
-
-
J. M. Mellor, N. M. Smith, J. Chem. Res. Synop. 1985, 60; J. M. Mellor, R. Pathirana, N. M. Smith, J. Chem. Soc. Perkin Trans. 1 1988, 2501.
-
(1988)
J. Chem. Soc. Perkin Trans. 1
, pp. 2501
-
-
Mellor, J.M.1
Pathirana, R.2
Smith, N.M.3
-
30
-
-
0001200668
-
-
G. Ritter, G. Häfelinger, E. Lüddecke, H. Rau, J. Am. Chem. Soc. 1989, 111, 4627; E. Tauer, K.-H. Grellmann, A. Heinrich, Chem. Ber. 1991, 124, 2053.
-
(1989)
J. Am. Chem. Soc.
, vol.111
, pp. 4627
-
-
Ritter, G.1
Häfelinger, G.2
Lüddecke, E.3
Rau, H.4
-
31
-
-
0010732916
-
-
G. Ritter, G. Häfelinger, E. Lüddecke, H. Rau, J. Am. Chem. Soc. 1989, 111, 4627; E. Tauer, K.-H. Grellmann, A. Heinrich, Chem. Ber. 1991, 124, 2053.
-
(1991)
Chem. Ber.
, vol.124
, pp. 2053
-
-
Tauer, E.1
Grellmann, K.-H.2
Heinrich, A.3
-
32
-
-
0842341771
-
-
AM1: M. J. S. Dewar, E. G. Zoebisch, E. F. Healy, J. J. P. Stewart, J. Am. Chem. Soc. 1985, 107, 3902; MM2: N. L. Allinger, H. C. Flanagan, J. Comput. Chem. 1983, 4, 399. For AM1 calculations MOPAC 6.0 was used.
-
(1985)
J. Am. Chem. Soc.
, vol.107
, pp. 3902
-
-
Dewar, M.J.S.1
Zoebisch, E.G.2
Healy, E.F.3
Stewart, J.J.P.4
-
33
-
-
84986495500
-
-
AM1: M. J. S. Dewar, E. G. Zoebisch, E. F. Healy, J. J. P. Stewart, J. Am. Chem. Soc. 1985, 107, 3902; MM2: N. L. Allinger, H. C. Flanagan, J. Comput. Chem. 1983, 4, 399. For AM1 calculations MOPAC 6.0 was used.
-
(1983)
J. Comput. Chem.
, vol.4
, pp. 399
-
-
Allinger, N.L.1
Flanagan, H.C.2
-
34
-
-
1542602080
-
-
P. S. Engel, Chem. Rev. 1980, 80, 99; M. A. Anderson, C. B. Grissom, J. Am. Chem. Soc. 1995, 117, 5041, and references therein.
-
(1980)
Chem. Rev.
, vol.80
, pp. 99
-
-
Engel, P.S.1
-
35
-
-
0000586215
-
-
and references therein
-
P. S. Engel, Chem. Rev. 1980, 80, 99; M. A. Anderson, C. B. Grissom, J. Am. Chem. Soc. 1995, 117, 5041, and references therein.
-
(1995)
J. Am. Chem. Soc.
, vol.117
, pp. 5041
-
-
Anderson, M.A.1
Grissom, C.B.2
-
36
-
-
0000358534
-
-
W. Adam, O. De Lucci, Angew. Chem. 1980, 92, 815; Angew. Chem. Int. Ed. Engl. 1980, 19, 762; W. Adam, G. Fragale, D. Klapstein, W. M. Nau, J. Wirz, J. Am. Chem. Soc. 1995, 117, 12578.
-
(1980)
Angew. Chem.
, vol.92
, pp. 815
-
-
Adam, W.1
De Lucci, O.2
-
37
-
-
0006911853
-
-
W. Adam, O. De Lucci, Angew. Chem. 1980, 92, 815; Angew. Chem. Int. Ed. Engl. 1980, 19, 762; W. Adam, G. Fragale, D. Klapstein, W. M. Nau, J. Wirz, J. Am. Chem. Soc. 1995, 117, 12578.
-
(1980)
Angew. Chem. Int. Ed. Engl.
, vol.19
, pp. 762
-
-
-
38
-
-
0029556376
-
-
W. Adam, O. De Lucci, Angew. Chem. 1980, 92, 815; Angew. Chem. Int. Ed. Engl. 1980, 19, 762; W. Adam, G. Fragale, D. Klapstein, W. M. Nau, J. Wirz, J. Am. Chem. Soc. 1995, 117, 12578.
-
(1995)
J. Am. Chem. Soc.
, vol.117
, pp. 12578
-
-
Adam, W.1
Fragale, G.2
Klapstein, D.3
Nau, W.M.4
Wirz, J.5
-
39
-
-
85033027458
-
-
note
-
13C decoupling experiments. Assignments marked by * may be interchanged as a whole set.
-
-
-
-
40
-
-
84989419224
-
-
In analogy the more reactive 4,4-dimethoxy-3,5-bistrifluoromethyl-4H-pyrazole (C. Gerninghaus, A. Kümmel, G. Seitz, Chem. Ber. 1993, 126, 733) underwent addition with cis-2 in boiling chlorobenzene (ca. 30% yield); however, neat hydrolysis of the adduct to the corresponding dialdehyde could not be effected. Cf. N. Bahr, Dissertation, University of Freiburg, 1994.
-
(1993)
Chem. Ber.
, vol.126
, pp. 733
-
-
Gerninghaus, C.1
Kümmel, A.2
Seitz, G.3
-
41
-
-
0001626316
-
-
-1); cf. K. Beck, S. Hünig, F.-G. Klärner, P. Kraft, U. Artschwager-Perl, Chem. Ber. 1987, 120, 2041.
-
(1987)
Chem. Ber.
, vol.120
, pp. 2041
-
-
Beck, K.1
Hünig, S.2
Klärner, F.-G.3
Kraft, P.4
Artschwager-Perl, U.5
-
42
-
-
33847804824
-
-
J. P. Snyder, V. T. Bandurco, F. Darack, H. Olsen, J. Am. Chem. Soc. 1974, 96, 5158.
-
(1974)
J. Am. Chem. Soc.
, vol.96
, pp. 5158
-
-
Snyder, J.P.1
Bandurco, V.T.2
Darack, F.3
Olsen, H.4
-
43
-
-
15744374710
-
-
Dissertation, University of Freiburg
-
G. Fischer, Dissertation, University of Freiburg, 1987.
-
(1987)
-
-
Fischer, G.1
-
44
-
-
85033013933
-
-
note
-
One of the remarkable chemical consequences of the special N=N/N=N arrangement in 8 is the stability of the 1,2,4,5-perhydrotetrazine formed after twofold methylation of 11 and base treatment in the presence of oxygen.
-
-
-
-
45
-
-
85033030177
-
-
note
-
-1 above 8A. Further details of the crystal structure investigation may be obtained from the Fachinformationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen (Germany), on quoting the depository number CSD-404417.
-
-
-
-
46
-
-
85033013333
-
-
Dissertation. University of Freiburg
-
K. Exner, Dissertation. University of Freiburg.
-
-
-
Exner, K.1
-
48
-
-
84985716577
-
-
Compare the rapid fragmentation of oxidized 1,2-diazetidines [5] and 1,2,3-triaziridines: W. Marterer, O. Klingler, R. Thiergardt, E. Beckmann, H. Fritz, H. Prinzbach, Chem. Ber. 1991, 124, 621.
-
(1991)
Chem. Ber.
, vol.124
, pp. 621
-
-
Marterer, W.1
Klingler, O.2
Thiergardt, R.3
Beckmann, E.4
Fritz, H.5
Prinzbach, H.6
|