Chiral discrimination of 1-phenylethylamine by diastereomeric salt formation with bile acids. Crystal structures of cholic acid salts with (R)- and (S)-1-phenylethylamine

Chemistry Letters

Volumn , Issue 10, 1996, Pages 837-838

  Sada, Kazuki ^a   Maeda, Tomohiro ^a   Miyata, Mikiji ^a  

^a OSAKA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0030372673     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1996.837     Document Type: Article

References (12)

1. J. Jacques, A. Collet, S. H. Wilen, "Enantiomers, Racemates, and Resolutions," John Wiley, New York (1981).
2. for examples, S. P. Zingg, E. M. Arnett, A. T. McPhail, A. A. Bothner-By, and W. R. Gilkerson, J. Am. Chem. Soc., 110, 1565 (1988), and references cited in; S. Larsen, and H. Lopez de Diego, J. Chem. Soc., Perkin Trans. 2, 1993, 469; K. Kinbara, Y. Hashimoto, M. Sukegawa, H. Nohira, and K. Saigo, J. Am. Chem. Soc., 118, 3441 (1996).
3. for examples, S. P. Zingg, E. M. Arnett, A. T. McPhail, A. A. Bothner-By, and W. R. Gilkerson, J. Am. Chem. Soc., 110, 1565 (1988), and references cited in; S. Larsen, and H. Lopez de Diego, J. Chem. Soc., Perkin Trans. 2, 1993, 469; K. Kinbara, Y. Hashimoto, M. Sukegawa, H. Nohira, and K. Saigo, J. Am. Chem. Soc., 118, 3441 (1996).
4. for examples, S. P. Zingg, E. M. Arnett, A. T. McPhail, A. A. Bothner-By, and W. R. Gilkerson, J. Am. Chem. Soc., 110, 1565 (1988), and references cited in; S. Larsen, and H. Lopez de Diego, J. Chem. Soc., Perkin Trans. 2, 1993, 469; K. Kinbara, Y. Hashimoto, M. Sukegawa, H. Nohira, and K. Saigo, J. Am. Chem. Soc., 118, 3441 (1996).
5. K. Miki, N. Kasai, M. Shibakami, K. Takemoto, and M. Miyata, J. Chem. Soc., Chem. Comm. 1991, 1757.
6. D. J. Collins and J. J. Hobbs, Aust. J. Chem., 23, 119 (1970); R. C. Kelly, I. Schletter, S. J. Stein, and W. Wierenga, J. Am. Chem. Soc., 101, 1054 (1979).
7. D. J. Collins and J. J. Hobbs, Aust. J. Chem., 23, 119 (1970); R. C. Kelly, I. Schletter, S. J. Stein, and W. Wierenga, J. Am. Chem. Soc., 101, 1054 (1979).
8. E. Giglio, "Inclusion Compounds," Academic Press, London (1984), Vol. 2, pp 207.
9. A. Ault, Org. Synth., 49, 93(1969).
10. -3, R=0.050, 1735 unique reflections with Fo>3σ(Fo).
11. -3, R=0.053, 2292 unique reflections with Fo>3σ(Fo).
12. -3, R=0.055, 1564 unique reflections with Fo>3σ(Fo).