ESR studies on poly(methyl acrylate) radicals to estimate their dominant structure

Chemistry Letters

Volumn , Issue 11, 1996, Pages 951-952

  Sugiyama, Yoshio ^a  

^a NIPPON STEEL CORPORATION   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0030363422     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1996.951     Document Type: Article

References (10)

1. J. G. Kloosterboer, G. F. C. M. Lijten, and F. J. A. M. Greidanus, Polym. Commun., 27, 268 (1986).
2. H. Yoshida, T. Kodaira, K. Tsuji, K. Hayashi, and S. Okamura, Bull. Chem. Soc. Jpn., 37, 1531 (1964).
3. P. Hesse, A. Rosenberg, and H. Heusinger, Eur. Polym. J., 9, 581 (1973).
4. G. Geuskens and C. David, Makromol. Chem., 165, 273 (1973).
5. J. A. Harris, O. Hinojosa, and J. C. Arthur, Jr., J. Polym. Sci., Polym., Chem., 12, 679 (1974).
6. H. Tanaka, T. Sato, and T. Otsu, Makromol. Chem., 180, 267 (1979).
7. 1H NMR (440 MHz, CCl4, relative to TMS) δ OCH3 3.71, δ Ha 5.77, δ Hb 6.34 ppm, JHa-Hb, 1.4, JHa-D 1.4, 7Hb-D 2.5 Hz; isotope (D) purity 97.9% by GC-mass, based on electron impact ioniization and selected ion monitoring techniques, comparing MA and MA-d.
8. K. Yokota, T. Hirabayashi, and K. Takahashi, Polym. J., 12, 177 (1980).
9. A. Carrington and A. D. McLachlan, in "Introduction to Magnetic Resonance," A Harper International Edition, Harper & Row, New York, Evanston & London, and John Weatherhill, Inc., Tokyo, (1967), Chap.6, (a)p15, 80, (b)p84.
10. M. E. Best and P. H. Kasai, Macromolecules, 22, 2622 (1989).