A new and effective synthesis of terminal alkylselenylacetylenes

Chinese Chemical Letters

Volumn 7, Issue 12, 1996, Pages 1085-1086

  Yang, De Yu ^a   Huang, Xian ^a   Li, Ping ^a  

^a ZHEJIANG UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0030353792     PISSN: 10018417     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (14)

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2. Brage, A.L., Reckziegel, A., Silveira, C.C.Synth.Comnnm. 1994,24,1165. Brage, A.L., Comasseto, J.V., Petagnai, N.Synthesis 1984, 240 comasseto, J.V., Catani, V., Ferreira, J.T.B., Brage, A.L., J.Chem.Soc., Chem.Commun. 1986,1067. Comasseto, J.V., Silveira, C.C.Ferreira, J.T.B., Catani, V.Synth. Commun. 1986, 16,283. Lang, H., Keller, H., Zmhof, W., Martin, S.Chem.Ber.1990, 123, 147.
3. Brage, A.L., Reckziegel, A., Silveira, C.C.Synth.Comnnm. 1994,24,1165. Brage, A.L., Comasseto, J.V., Petagnai, N.Synthesis 1984, 240 comasseto, J.V., Catani, V., Ferreira, J.T.B., Brage, A.L., J.Chem.Soc., Chem.Commun. 1986,1067. Comasseto, J.V., Silveira, C.C.Ferreira, J.T.B., Catani, V.Synth. Commun. 1986, 16,283. Lang, H., Keller, H., Zmhof, W., Martin, S.Chem.Ber.1990, 123, 147.
4. Brage, A.L., Reckziegel, A., Silveira, C.C.Synth.Comnnm. 1994,24,1165. Brage, A.L., Comasseto, J.V., Petagnai, N.Synthesis 1984, 240 comasseto, J.V., Catani, V., Ferreira, J.T.B., Brage, A.L., J.Chem.Soc., Chem.Commun. 1986,1067. Comasseto, J.V., Silveira, C.C.Ferreira, J.T.B., Catani, V.Synth. Commun. 1986, 16,283. Lang, H., Keller, H., Zmhof, W., Martin, S.Chem.Ber.1990, 123, 147.
5. Brage, A.L., Reckziegel, A., Silveira, C.C.Synth.Comnnm. 1994,24,1165. Brage, A.L., Comasseto, J.V., Petagnai, N.Synthesis 1984, 240 comasseto, J.V., Catani, V., Ferreira, J.T.B., Brage, A.L., J.Chem.Soc., Chem.Commun. 1986,1067. Comasseto, J.V., Silveira, C.C.Ferreira, J.T.B., Catani, V.Synth. Commun. 1986, 16,283. Lang, H., Keller, H., Zmhof, W., Martin, S.Chem.Ber.1990, 123, 147.
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9. In the application of intenal acetylenic selenide, we found that hydroboration of this acetylenic selenide with dialkylborane resulted in two isomers. which appeared to be poor regioselective.
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14. 1 (20 mmol) was slowly added to a cold (-20 'C),stirred 2 (20 mmol) over 1 h under the condition of N2.