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Volumn 116, Issue , 1996, Pages 77-92

Synthesis and characterization of terminally functionalized n-alkanethiols

Author keywords

Interfacial crystal growth; Long chain alkane thiols; Molecular crystals; Self assembled monolayers

Indexed keywords


EID: 0030327733     PISSN: 10426507     EISSN: None     Source Type: Journal    
DOI: 10.1080/10426509608040471     Document Type: Article
Times cited : (12)

References (42)
  • 1
    • 0003519909 scopus 로고
    • Academic Press: San Diego, CA
    • A., Ulman, An Introduction to Ultrathin Films, (Academic Press: San Diego, CA, 1991); Israelachvili, Intermolecular and Surface Forces, 2nd ed. (Academic Press: San Diego, CA, 1992).
    • (1991) An Introduction to Ultrathin Films
    • Ulman, A.1
  • 2
    • 84961911284 scopus 로고
    • Academic Press: San Diego, CA
    • A., Ulman, An Introduction to Ultrathin Films, (Academic Press: San Diego, CA, 1991); Israelachvili, Intermolecular and Surface Forces, 2nd ed. (Academic Press: San Diego, CA, 1992).
    • (1992) Israelachvili, Intermolecular and Surface Forces, 2nd Ed.
  • 21
    • 0025401950 scopus 로고
    • 1 NMR data. We were able to obtain 11-mercaptoundecanoic acid as a white crystalline solid which melts at 40-41°C, and 11-mercaptoundecanol as an off-white crystalline material which melts at 34-35°C (both pure by H1 NMR and elemental analyses). See: C. E. D. Chidsey, et al. Langmuir, 6, 682, (1990).
    • (1990) Langmuir , vol.6 , pp. 682
    • Chidsey, C.E.D.1
  • 23
    • 0001622541 scopus 로고
    • T. Kolasa and M. J. Miller, J. Org. Chem., 55, 1711, (1990); G. C. Harrison, H. Diehl, Organic Syntheses; Wiley: New York, Collect. Vol. 3, 370, (1965).
    • (1990) J. Org. Chem. , vol.55 , pp. 1711
    • Kolasa, T.1    Miller, M.J.2
  • 24
    • 0001622541 scopus 로고
    • Wiley: New York, Collect.
    • T. Kolasa and M. J. Miller, J. Org. Chem., 55, 1711, (1990); G. C. Harrison, H. Diehl, Organic Syntheses; Wiley: New York, Collect. Vol. 3, 370, (1965).
    • (1965) Organic Syntheses , vol.3 , pp. 370
    • Harrison, G.C.1    Diehl, H.2
  • 26
    • 0041665619 scopus 로고    scopus 로고
    • Ethanol can be used instead to improve solubility of the bromide if necessary
    • Ethanol can be used instead to improve solubility of the bromide if necessary.
  • 28
    • 0002971520 scopus 로고
    • J. A. Birch and G. S. Rao, Adv. Org. Chem., 8, 1, (1972); J. A. Birch, A. L. Hinde and L. Radom, J. Am. Chem. Soc., 102, 3370, (1980).
    • (1972) Adv. Org. Chem. , vol.8 , pp. 1
    • Birch, J.A.1    Rao, G.S.2
  • 37
    • 0043168592 scopus 로고    scopus 로고
    • Other members of this series have also been prepared but gave unsatisfactory elemental analyses. We are in the process of developing methods to prepare these materials in better yields and higher quality
    • Other members of this series have also been prepared but gave unsatisfactory elemental analyses. We are in the process of developing methods to prepare these materials in better yields and higher quality
  • 39
    • 0042667598 scopus 로고    scopus 로고
    • Private communications with S. Ohara, M. Kitamura, K. Takahashi, and M. Kondo of Hitachi Research Laboratory, Japan
    • Private communications with S. Ohara, M. Kitamura, K. Takahashi, and M. Kondo of Hitachi Research Laboratory, Japan.
  • 40
    • 0043168591 scopus 로고    scopus 로고
    • The reflux period required for complete reaction varies considerably with the identity of the halide, most bromides require about 3 hours
    • The reflux period required for complete reaction varies considerably with the identity of the halide, most bromides require about 3 hours.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.