Reactions of (CF3)2BNMe2 with Grignard and related reagents. Crystal and molecular structure of (CF3)(Mes)FB-FC=NMe2 and Ph3P-CH2-(CF3)2B-NMe2 1

Journal of Organometallic Chemistry

Volumn 524, Issue 1-2, 1996, Pages 225-235

  Brauer, David J ^a   Bürger, Hans ^a   Dittmar, Thomas ^a   Pawelke, Gottfried ^a   Rothe, Jürgen ^a  

^a UNIVERSITY OF WUPPERTAL   (Germany)

Author keywords

Boron; Dimethylaminobis(trifluoromethyl)borane; Grignard reagents

Indexed keywords

EID: 0030295590     PISSN: 0022328X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-328X(96)06400-5     Document Type: Article

References (24)

1. [1] G. Pawelke and H. Bürger, Appl. Organomet. Chem., 10 (1996) 147.
2. [2] A. Ansorge, D.J. Brauer, H. Bürger, T. Hagen and G. Pawelke, J. Organomet. Chem., 444 (1993) 5.
3. [3] H. Bürger, G. Pawelke and J. Rothe, J. Organomet. Chem., 474 (1994) 43.
4. [4] H. Bürger, T. Hagen and G. Pawelke, J. Organomet. Chem., 456 (1993) 19.
5. [5] D. Seyferth and S.O. Grim, J. Am. Chem. Soc., 83 (1961) 1613.
6. [6] R. Köster and B. Rickborn, J. Am. Chem. Soc., 89 (1967) 2782.
7. [7] A. Ansorge, D.J. Brauer, H. Bürger, F. Dörrenbach, B. Krumm and G. Pawelke Z. Naturforsch. Teil B:, 47 (1992) 772.
8. [8] R. Taube, S. Wache and J. Sieler, J. Organomet. Chem., 459 (1993) 335.
9. [9] D.J. Brauer, H. Bürger and G. Pawelke, J. Organomet. Chem., 238 (1982) 267.
10. [10] G. Brunton, Acta Crystallogr. Sect. B:, 25 (1969) 2161.
11. [11] D.J. Brauer, H. Bürger and G. Pawelke, Inorg. Chem., 16 (1977) 2305.
12. [12] D.J. Brauer, H. Bürger and G. Pawelke, J. Organomet. Chem., 192 (1980) 305.
13. [13] A. Ansorge, D.J. Brauer, H. Bürger, T. Hagen and G. Pawelke, J. Organomet. Chem., 467 (1994) 1.
14. [14] J.C.T. Bart, J. Chem. Soc. B., (1969) 350.
15. [15] R. Hausser-Wallis, H. Oberhammer, H. Bürger and G. Pawelke, J. Chem. Soc. Dalton Trans., (1987) 1839.
16. [16] A. Ansorge, D.J. Brauer, S. Buchheim-Spiegel, H. Bürger, T. Hagen and G. Pawelke, J. Organomet. Chem., 501 (1995) 347.
17. [17] D. Naumann and W. Tyrra, J. Chem. Soc. Chem. Commun., (1989) 47.
18. 13C-NMR-Spektroskopie Georg Thieme, Stuttgart 1984.,
19. [19] K. Burger and B. Helmreich, J. Chem. Soc. Chem. Comm., (1992) 348.
20. [20] E. Sattler, in R. Köster (ed.), (Houben-Weyl) Organoborverbindungen, Vol. 13/3b, Georg Thieme, Stuttgart, 4th edn., 1983, p. 470.
21. [21] A. Ansorge, D.J. Brauer, H. Bürger, T. Hagen and G. Pawelke, Angew. Chem., 105 (1993) 429.
22. [22] K. Jones and M.F. Lappert, J. Organomet. Chem., 3 (1965) 295.
23. [23] G.M. Sheldrick, SHELXS-86: program for crystal structure solutions, University of Göttingen, 1986.
24. [24] G.M. Sheldrick, SHELX-76: program for crystal structure determination, University of Cambridge, 1976.