Resolution of cis-4-O-TBS-2-cyclopenten-1,4-diol

Tetrahedron Asymmetry

Volumn 7, Issue 10, 1996, Pages 2791-2792

  Curran, Timothy T ^a,b   Hay, David A ^a  

^a SANOFI   (France)

^b PFIZER INC   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

2 CYCLOPENTENE 1,4 DIOL DERIVATIVE; CYCLOALKANOL DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; DRUG PURIFICATION; ENANTIOMER; ENZYME ACTIVITY; NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL;

EID: 0030272826     PISSN: 09574166     EISSN: None     Source Type: Journal    
DOI: 10.1016/0957-4166(96)00363-1     Document Type: Article

References (17)

1. 1. a) Theil, F.; Schick, H.; Lapitskaya, M.A. and Pivnitsky, K. K. Liebigs. Ann. Chem. 1991, 195-200.
2. b) Theil, F.; Schick, H.; Weichert, D.; Tannenberger, K. and Klappach, G. J. Prakt. Chem. 1991, 333, 497-499.
3. c) Theil, F.; Schick, H.; Winter, G. and Reck, G. Tetrahedron 1991, 47, 7569-7582.
4. d) Johnson, C. R. and Bis, S. J. Tetrahedron Lett. 1992, 33, 7287-7290.
5. e) Deardorff, D. R.; Windham, C. Q. and Craney, C. L. Org. Synth. 1995, 73, 25-35.
6. f) Washausen, P.; Grebe, H.; Kieslich, K. and Winterfeldt, E. Tetrahedron Lett. 1989, 30, 3777-3778.
7. g) Paquette, L. A.; Earle, M. J. and Smith, G. F. Org. Synth. 1995, 73, 36-43.
8. h) ibid., 44-49.
9. i) Myers, A. G.; Hammond, M. and Wu, Y. Tetrahedron Lett. 1996, 37, 3083-3086.
10. j) Schoffers, E.; Golebiowski, A. and Johnson, C. R. Tetrahedron 1996, 52, 3769-3826.
11. k) Laumen K. and Schneider, M. Tetrahedron Lett. 1984, 25, 5875.
12. 2. Collins, P.W. and Djuric, S. W. Chem. Rev. 1993, 93, 1533-1564.
13. 3. a) Borthwick, A. D. and Biggadike, K. Tetrahedron 1992, 48, 571-623.
14. b) Dyatkina, N.; Costisella, B.; Theil, F. and von Janta-Lipinski, M. Tetrahedron Lett. 1994, 35, 1961-1964.
15. 4. Toyota, A.; Katagiri, N. and Kaneko, C. Chem Pharm. Bull. 1992, 40, 1039-1041. A newly-developed route to compound 1 and full details on the resolution of similar compounds will be reported in due course.
16. 13C NMR, IR, MS) and were at least 98% pure by GC.
17. R (3) = 17.47 min.