Confirmatory mass-spectral data for cyclic fatty acid monomers

JAOCS, Journal of the American Oil Chemists' Society

Volumn 73, Issue 10, 1996, Pages 1317-1321

  Mossoba, M M ^a   Yurawecz, P M ^a   Roach, J A G ^a   McDonald, R E ^a   Perkins, E G ^b  

^a CENTER FOR DRUG EVALUATION AND RESEARCH   (United States)

^b UNIVERSITY OF ILLINOIS AT URBANA CHAMPAIGN   (United States)

Author keywords

2 Alkyl 4,4 dimethyloxazoline; Cyclic fatty acid monomers; Electron ionization mass spectrometry; Gas chromatography

Indexed keywords

EID: 0030269447     PISSN: 0003021X     EISSN: None     Source Type: Journal    
DOI: 10.1007/BF02525462     Document Type: Article

References (16)

1. Crampton, E.W., R.H. Common, E.T. Pritchard, and F.A. Farmer, Studies to Determine the Nature of the Damage to the Nutritive Value of Some Vegetable Oils from Heat Treatment, J. Nutr. 60:13-24 (1956).
2. Iwaoka, W.T., and E.G. Perkins, Nutritional Effects of the Cyclic Monomers of Methyl Linolenate in the Rat, Lipids 11:349-353 (1976).
3. Iwaoka, W.T., and E.G. Perkins, Metabolism and Lipogenic Effects of the Cyclic Monomers of Methyl Linolinate in the Rat, J. Am. Oil Chem. Soc. 55:734-738 (1978).
4. Sebedio, J.L., and A. Grandgirard, Cyclic Fatty Acids: Natural Sources, Formation during Heat Treatment, Synthesis and Biological Properties, Prog. Lipid Res. 28:303-336 (1989).
5. Mossoba, M.M., M.P. Yurawecz, J.A.G. Roach, H.S. Lin., R.E. McDonald, B.D. Flickinger, and E.G. Perkins, Rapid Determination of Double Bond Configuration and Position Along the Hydrocarbon Chain in Cyclic Fatty Acid Monomers, Lipids. 29:893-896 (1994).
6. Dobson, G., W.W. Christie, E.Y. Brechany, J.L. Sebedio, and J.L. Le Quere, Silver Ion Chromatography and Gas Chromatography-Mass Spectrometry in the Structural Analysis of Cyclic Dienoic Acids Formed in Frying Oils, Chem. Phys. Lipids 75:171-182 (1995).
7. Mossoba, M.M., M.P. Yurawecz, J.A.G. Roach, H.S. Lin.., R.E. McDonald, B.D. Flickinger, and E.G. Perkins, Elucidation of Cyclic Fatty Acid Monomer Structures. Cyclic and Bicyclic Ring Sizes and Double Bond Position and Configuration, J. Am. Oil Chem. Soc. 72:721-727 (1995).
8. Mossoba, M.M., M.P. Yurawecz, J.A.G. Roach, R.E. McDonald, B.D. Flickinger, E.G. Perkins, Application of GC-MI-FTIR Spectroscopy to the Structural Elucidation of Cyclic Fatty Acid Monomers, Am. Lab. (Shelton, Conn.). 27:16K-O (1995).
9. Zhang, J.Y., Q.T. Yu, B.N. Liu, and Z.H. Huang, Chemical Modification in Mass Spectrometry IV. 2-Alkenyl-4,4-Dimethyloxazolines as Derivatives for Double Bond Location of Long-Chain Olefinic Acids, Biomed. and Environ. Mass Spec. 15:33-44 (1988).
10. Fay, L., and U. Richly, Location of Double Bonds in Polyunsaturated Fatty Acids by Gas Chromatography-Mass Spectrometry After 4,4-Dimethyloxazoline Derivatization, J. Chromatogr. 541:89-98 (1991).
11. Bourne, S., G. Reedy, P. Coffey, and D. Mattson, Matrix Isolation GC-FTIR, Am. Lab. (Shelton, Conn.) 16:90-101 (1984).
12. Reedy, G.T., D.C. Ettinger, J.F. Schneider, and S. Bourne, High Resolution Gas Chromatography/Matrix Isolation Infrared Spectrometry, Anal. Chem. 57:1602-1609 (1985).
13. Sebedio, J.L., J. Prevost, and A. Grandgirard, Heat Treatment of Vegetable Oils I. Isolation of the Cyclic Fatty Acid Monomers from Heated Sunflower and Linseed Oils, J. Am. Oil Chem. Soc. 64:1026-1032 (1987).
14. Rojo, J.A., and E.G. Perkins, Cyclic Fatty Acid Monomer Formation in Frying Fats. I. Determination and Structural Study, Ibid. 64:414-421 (1987).
15. Rakoff, H., and E.A. Emken, Syntheses of Geometric Isomers of Di-. Tetra-, and Hexadeuterated 12-Octadecenoates and Their Triglycerides, J. Labelled Comp. Radiopharm. 15:233-252 (1978).
16. Hase, A., A. Kaltia, M.A. Matikainen, and T. Hase, Cyclopinolenic Acids: Synthesis, Derivatives and Thermal Properties, J. Am. Oil Chem. Soc. 69:1027-1031 (1992).