Identification and Quantitation of Oxygenates in Gasoline Ampules Using Fourier Transform Near-Infrared and Fourier Transform Raman Spectroscopy

Analytical Chemistry

Volumn 68, Issue 20, 1996, Pages 3525-3533

  Choquette, Steven J ^a   Chesler, Stephen N ^a   Duewer, David L ^a   Wang, Shuwen ^b   O'Haver, Thomas C ^b  

^a NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

^b Bldg 142   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CHEMICAL ANALYSIS; ETHANOL; FOURIER TRANSFORM INFRARED SPECTROSCOPY; GASOLINE; ORGANIC COMPOUNDS; RAMAN SPECTROSCOPY;

ETHYL TERT-BUTYL ETHERS; IDENTIFICATION; METHYL TERT-BUTYL ETHERS; OXYGENATES; STANDARD REFERENCE MATERIALS; TERT-AMYL METHYL ETHERS;

ETHERS;

EID: 0030261740     PISSN: 00032700     EISSN: None     Source Type: Journal    
DOI: 10.1021/ac960451v     Document Type: Article

References (33)

1. Gurney, J. Petroleum Rev. 1993, May, 229-231.
2. Verga G. R.; Sironi, A.; Schneider, W.; Frohne, Ch. J. HRC & CC 1988, 11248.
3. Dechl, J. W.; Finkbeiner, J. W.; DiSanzo, F. P. Anal. Chem. 1992, 64, 3202.
4. Goode, S. R.; Thomas, C. L. J. Anal. At. Spectrom. 1994, 9, 73-78.
5. McNamara, E. A.; Montzka, S. A.; Berkley, R M.; Silvers, R. E. J. Chromatogr. 1988, 452, 75-83.
6. Sadeghi-Jorabchi, H.; Wilson, R. H.; Belton, P. S.; Edwards-Webb, J. D.; Coxon, D. T. Spectrochim. Acta 1991, 47A (9/10), 1449-1458.
7. 2, of the measurements. The expanded uncertainty is the total combined uncertainty multiplied by a coverage factor of 2. All measurement uncertainties are calculated in accord with NIST Technical Note 1297: Guidelines for Evaluation and Expressing the Uncertainty of NIST Measurementment Results; Taylor, B. N., Kuyatt, C. E., Eds.; U.S. Government Printing Office: Washington, DC, 1994.
8. Buchanan, B. R.; Honigs, D. E. Appl. Spectrosc. 1987, 41 (8), 1388-1392.
9. Garcia, F. X.; Lima, L. D.; Medina, J. C. Appl. Spectrosc. 1993, 47 (7), 1036-1039.
10. Kelly, J. J.; Barlow, C. H.; Jinguji, T. M.; Callis, J. B. Anal. Chem. 1989, 61, 313-320.
11. Parisi, A. F.; Nogueiras, L.; Prieto, H. Anal. Chim. Acta 1990, 238, 95-100.
12. Kelly, J. J.; Callis, J. B. Anal. Chem. 1990, 62, 1444-1451.
13. Swarin, S. J.; Drumm, C. A. Spectroscopy 1992, 7 (7), 42-46.
14. Wong, J. L.; Jaselskis, B. Analyst, 1982, 107, 1282.
15. DeSimas, B. D.; Lane, L. Measurement of MTBE in Gasolines by NIR; ISA Paper 90-462 Instrument Society of America: Research Triangle Park, NC, 1990.
16. Seasholtz, M. B.; Archibard, D. D.; Lorber, A.; Kowalski, B. R. Appl. Spectrosc. 1989, 43 (6), 1067-1072.
17. Cooper, J. B.; Wise, K. L.; Groves, J.; Welch, W. T. Anal. Chem. 1995, 67, 4096-4100.
18. Cooper, J. H.; Flecher, P. E.; Vess, T. M.; Welch, W. Appl. Spectrosc. 1995, 49 (5), 586-592.
19. Martens, H.; Naes, T. Multivariate Calibration; Wiley: New York, 1989.
20. Sjöström, M.; Wold, S.; Lindberg, W.; Persson, J. A.; Martens, H. Anal. Chim. Acta 1983, 150, 61-70.
21. Certain commercial equipment, instruments, and materials are identified in this paper in order to specify the experimental procedure as completely as possible. In no case does such identification imply a recommendation or endorsement by the National Institute of Standards and Technology, nor does it imply that the material, instrument, or equipment is necessarily the best available for the purpose.
22. Chesler, S. N.; Green, T. L.; Duewer, D. L.; Guenther, F. R.; May, W. E. Certification of SRMs 2293, 2292, 2291, 2290, 2289, 2288 and NTRMs 82293, 82292, 82291, 82290, 82289, 82288 Ether Oxygenates in Gasoline; Report of Analysis 835-94-109; Analytical Chemistry Division, 222/B324; NIST: Gaithersburg, MD, 20-Sep-94.
23. Chesler, S. N.; Green, T. L.; Duewer, D. L.; Guenther, F. R.; May, W. E. Certification of SRMs 2287, 2286 and NTRMs 82287, 82286 Ethanol in Gasoline; Report of Analysis 835-94-108; Analytical Chemistry Division, 222/ B324; NIST: Gaithersburg, MD, 26-Sep-94.
24. Wheeler, O. H. Chem. Rev. 1959, 59, 629-666.
25. Evans, A.; Hibbard, R. R.; Powell, A. S. Anal. Chem. 1951, 23, 1604-1610.
26. Weyer, L. G. Appl. Spectrosc. Rev. 1985, 21 (1&2), 1-43.
27. Lin-Vien, D.; Colthup, N. B.; Fateley, W. G.; Grasselli, J. G. The Handbook of Infrared and Raman characteristic Frequencies of Organic Molecules; Academic Press, Inc.: New York, 1991.
28. Dollish, F. R.; Fateley, W. G.; Bentley, F. F. Characteristic Raman frequency of Organic Compounds; 1973.
29. OPUS/IR Reference Manual; Bruker Billerica, MA, 1995.
30. Geladi, P.; MacDougall, D.; Martens, H. Appl. Spectrosc. 1985, 39, 491.
31. Miller, C. Spectrochim. Acta 1993, 49A, 621-632.
32. Private communication, Dr. Klaas Farber, Center for Process Analytical Chemistry, University of Washington, Seattle, WA.
33. Everall, N. J. Raman Spectrosc. 1994, 25, 813-819.