An improved, two step synthesis of the chiral templating reagent 2,6-Dihydroxy-9,10-dihydro-11,12-dicarbomethoxyethenoanthracene

Tetrahedron Asymmetry

Volumn 7, Issue 8, 1996, Pages 2407-2410

  Adrian Jr , James C ^a   Ovitt, Tina M ^a  

^a UNION COLLEGE   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ANTHRACENE DERIVATIVE;

ARTICLE; CHIRALITY; DRUG STRUCTURE; DRUG SYNTHESIS; NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL; TECHNIQUE;

EID: 0030221455     PISSN: 09574166     EISSN: None     Source Type: Journal    
DOI: 10.1016/0957-4166(96)00298-4     Document Type: Article

References (5)

1. 1. Wilcox, C. S.; Greer, L. M.; Lynch, V. J. Am. Chem. Soc. 1987, 109, 1865-1867.
2. 2. (a) Petti, M. A.; Shepodd, T. J.; Barrans, R. E.; Dougherty, D. A. J. Am. Chem. Soc. 1988, 110, 6825-6870.
3. (b) Webb, T. H.; Suh, H.; Wilcox, C. S. J. Am. Chem. Soc. 1991, 113, 8554-8555.
4. 3. The DMnAD was prepared according to the method of Charlton on a 15 g scale in four steps, in an overall 70% yield: Charlton, J. L.; Chee, G. Tetrahedron Lett. 1994, 35, 6243-6246.
5. 4. Still, W. C.; Khan, M., Mitra, A. J. Org. Chem. 1978, 43, 2923-2925.