A gas-to-solid phase methanolysis method for the analysis of small amounts of oligosaccharides

Canadian Journal of Chemistry

Volumn 74, Issue 8, 1996, Pages 1512-1523

  Asres, Daniel Derbie ^a   Perreault, Hélène ^a  

^a UNIVERSITY OF MANITOBA   (Canada)

Author keywords

Gas chromatography Mass spectrometry; Mass spectrometry; Methanolysis; Oligosaccharides; Permethylation

Indexed keywords

GAS CHROMATOGRAPHY; MASS SPECTROMETRY; MOLECULAR STRUCTURE; PHASE TRANSITIONS; REACTION KINETICS; SACCHARIFICATION;

METHANOLYSIS; OLIGOSACCHARIDES; PERMETHYLATION;

SUGARS;

EID: 0030218142     PISSN: 00084042     EISSN: None     Source Type: Journal    
DOI: 10.1139/v96-168     Document Type: Article

References (19)

1. W.J. Richter, D.T. Müller, and B. Domon. Methods Enzymol. 193, 607 (1990).
2. H. Perreault, O. Koul, J. Street, R.H. McCluer, and C.E. Costello. Proc. 43rd Conf. Mass Spectrom. Allied Topics, May 21-26, 1995, Atlanta, Ga. p. 1179.
3. H. Perreault and C.E. Costello. Can. J. Chem. In press.
4. V.N. Reinhold, B.B. Reinhold, and C.E. Costello. Anal. Chem. 67, 1772 (1995).
5. H. Perreault and C.E. Costello. Org. Mass Spectrom. 29, 720 (1994).
6. A.S. Angel and B. Nilsson. Biomed. Environ. Mass Spectrom. 21, 202 (1992).
7. B. Fournet, G. Strecker, Y. Leroy, and J. Montreuil. Anal. Biochem. 116, 489 (1981).
8. A. Dell, N.H. Carman, P.R. Tiller, and J.E. Thomas-Oates. Biomed. Environ. Mass Spectrom. 16, 19 (1988).
9. A. Dell. Methods Enzymol. 193, 647 (1990).
10. C.C. Sweeley, R. Bentley, M. Makita, and W.W. Wells. J. Am. Chem. Soc. 85, 2497 (1963).
11. G. Larsson, H. Karlsson, G.C. Hansson, and W. Pimlott. Carbohydr. Res. 161, 281 (1987).
12. B. Domon, D.R. Müller, and W.J. Richter. Org. Mass Spectrom. 29, 715 (1994).
13. M.D. Ullman and R.H. McCluer. J. Lipid Res. 26, 501 (1985).
14. S.K. Gross and R.H. McCluer. Anal. Biochem. 102, 429 (1980).
15. K. Nishimura and K. Nakamura. J. Biochem. 98, 1247 (1985).
16. J.E. Vath. Ph.D. Thesis, Massachusetts Institute of Technology, 1990.
17. B. Domon, J.E. Vath, and C.E. Costello. Anal. Biochem. 184, 151 (1990).
18. C.E. Costello and J.E. Vath. Methods Enzymol. 193, 738 (1990).
19. NIST Standard Reference Database, Series 1a, NIST/EPA/NIH Database Version 4.5, February 1994, U.S. Department of Commerce. (a) α-D-Galactopyranoside, methyl 2,3,4,6-tetra-O-methyl-. CAS no.: 3149-64-2, EPA no.: 22952, DB no.: 21122. (b) β-D-Galactopyranoside, methyl 2,3,4,6-tetra-O-methyl-. CAS no.: 2296-47-1, EPA no.: 31190, DB no. 21127. (c) D-Galactopyranose, 2,3,4,6-tetra-O-methyl-. CAS no.: 3353-52-4, EPA no.: 31194, DB no.: 7138. (d) α-D-Glucopyranoside, methyl 2,3,4,6-tetra-O-methyl-. CAS no.: 605-81-2, EPA no.: 101817, DB no.: 22124. (e) β-D-Glucopyranoside, methyl 2,3,4,6-tetra-tetra-O-methyl-. CAS no.: 3149-65-3, EPA no.: 33672, DB no.: 21248. (f) α-D-Mannopyranoside, methyl 2,3,4-tri-O-methyl-6-deoxy. CAS no.: 72983-16-5, EPA no.: 101806, DB no.: 21125. (g) β-D-Mannopyranoside, methyl 2,3,4-tri-O-methyl-6-deoxy. CAS no.: 35939-74-3, EPA no.: 101807, DB no.: 21113. (h) α-D-Glucopyranoside, 2,3,4,6-tetra-O-methyl-α-D-glucopyranosyl 2,3,4,6-tetra-O-methyl. CAS no.: 25018-29-5, EPA no.: 17735, DB no.: 25394. (i) D-Glucopyranose, 2,3,4,6-tetra-O-methyl-. CAS no.: 7506-68-5, EPA no.: 31193, DB no.: 7137.