The formation of 1,2-propadiene-1,3-dithione (carbon subsulfide) from flash vacuum pyrolysis of 1,2-dithiole-3-thiones

Tetrahedron Letters

Volumn 37, Issue 27, 1996, Pages 4805-4808

  Pedersen, Carl Th ^a  

^a UNIVERSITY OF SOUTHERN DENMARK   (Denmark)

Author keywords

[No Author keywords available]

Indexed keywords

1,2 DITHIOLE 3 THIONE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; INFRARED SPECTROPHOTOMETRY; PYROLYSIS; REACTION ANALYSIS;

EID: 0030200125     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)00941-0     Document Type: Article

References (16)

1. 1. (a) Stadlbauer, W and Kappe, Th. Chem.-Ztg. 1977, 101, 137-141.
2. (b) Mihály, T. B. and Kauffman, G. B. Polyhedron, 1985, 4, 775-781.
3. (c) Schaumann, E. In Methoden Org. Chem. (Houben-Weyl) 1985, Vol. E11, Thieme Verlag, Stuttgart 1985, 232-233.
4. 2. (a) Kappe, Th. and Ziegler, E. Angew. Chem., 1974, 86, 529-42.
5. (b) Kappe, Th. In Methoden Org. Chem. (Houben-Weyl) 1993, Vol. E15, Thieme Verlag, Stuttgart 1993, 3119-3145.
6. 3. Stadlbauer, W.; Kappe, Th. and Ziegler, E. Z. Naturforsch., B, 1977, 32B, 893-897.
7. 4. Stadlbauer, W.; Kappe, Th. and Ziegler, E. Z. Naturforsch., B, 1978, 33B, 89-93.
8. 5. Kappe, C. O.; Pedersen, C. Th.; Catel, J. -M. and Mollier, Y. J. Chem. Soc., Perkin Trans. 2, 1994, 351-355.
9. 6. Pedersen, C. Th. and Kappe, C. O. Phosphorus Sulfur, 1994, 95-96, 485-486.
10. 2 formed in the pyrolysis.
11. 8. Takeuchi, N. and Tasumi M. J. Mol. Spectrosc., 1981, 90, 116.
12. 9. Wong, M. W.; Wentrup, C. and Flammang, R. J. Phys. Chem., 1995, 99, 16849-16856.
13. 10. Pedersen. C. Th.; Oddershede, J. and Sabin, J. R. J. Chem. Soc., Perkin Trans. 2,1981,1062-1065.
14. 11. The dithiole-3-thiones pyrolysed were prepared by conventional methods cf. ref. 12 and 13.
15. 12. Pedersen, C. Th. Adv. Heterocycl. Chem., 1982, 31, 63-113.
16. 13. Pedersen, C. Th. Sulfur Reports, 1995, 16, 173-221.