Spectral editing in 13C CP/MAS experiments at high magnetic field

Solid State Nuclear Magnetic Resonance

Volumn 6, Issue 2, 1996, Pages 187-196

  Hu, Jian Zhi ^a   Wu, Xiaoling ^a,c   Yang, Nianhua ^a   Li, Liyun ^a   Ye, Chaohui ^a   Qin, Kuangzong ^b  

^a Wuhan National Laboratory for Optoelectronics   (China)

^b CHINA UNIVERSITY OF PETROLEUM   (China)

^c YALE UNIVERSITY   (United States)

Author keywords

13C CP MAS spectral editing; High magnetic field; Slow MAS; TOSS

Indexed keywords

CARBON; ETHYL FUMARATE; FUMARIC ACID DERIVATIVE;

ANISOTROPY; ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; MAGNETISM; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ANISOTROPY; CARBON ISOTOPES; FUMARATES; MAGNETIC RESONANCE SPECTROSCOPY; MAGNETICS; MOLECULAR STRUCTURE;

ANISOTROPY; BAND STRUCTURE; CARBON; CHEMICAL REACTIONS; ESTERS; MAGNETIC FIELDS; MAGNETIC VARIABLES MEASUREMENT; POLARIZATION; SIGNAL DISTORTION;

ALIPHATIC CARBON ATOMS; CARBON CROSS POLARIZATION; CHEMICAL SHIFT ANISOTROPIES; FUMARIC ACID MONOETHYL ESTER; MAGIC ANGLE SPINNING; SIGNAL INTENSITY DISTORTION; SPECTRAL EDITING; TOTAL SIDE BAND SUPPRESSION PULSE SEQUENCE;

SPECTRUM ANALYSIS;

EID: 0030111932     PISSN: 09262040     EISSN: None     Source Type: Journal    
DOI: 10.1016/0926-2040(95)01203-6     Document Type: Article

References (47)

1. S.R. Hartman and E.L. Hann, Phys. Rev., 128 (1962) 2042.
2. A. Pines, M.G. Gibby and J.S. Waugh, J. Chem. Phys., 56 (1972) 1776; 59 (1973) 569; Chem. Phys. Lett., 15 (1972) 373.
3. A. Pines, M.G. Gibby and J.S. Waugh, J. Chem. Phys., 56 (1972) 1776; 59 (1973) 569; Chem. Phys. Lett., 15 (1972) 373.
4. A. Pines, M.G. Gibby and J.S. Waugh, J. Chem. Phys., 56 (1972) 1776; 59 (1973) 569; Chem. Phys. Lett., 15 (1972) 373.
5. (a) E.R. Andrew, A. Bradbury and R.G. Eades, Nature, 182 (1958) 1659.
6. (b) I.J. Lowe, Phys. Rev. Lett., 2 (1959) 285.
7. J.F. Shaefer and E.O. Stejskal, J. Am. Chem. Soc., 98 (1976) 1031.
8. D.T. Pegg, D.M. Doddrel and M.R. Bendall, J. Chem. Phys., 77 (1982) 2745.
9. R.R. Ernst, G. Bodenhausen and A. Wokaun, Principles of Nuclear Magnetic Resonance in One and Two Dimensions, International Series of Monographs on Chemistry, Oxford University Press, New York, 1987.
10. T. Terao, H. Miura and A. Saika, J. Chem. Phys., 75 (1981) 1573.
11. K.W. Zilm and D.M. Grant, J. Magn. Reson., 48 (1982) 524.
12. T. Terao, H. Miura and A. Saika, J. Magn. Reson., 49 (1982) 365.
13. T. Terao, H. Miura and A. Saika, J. Am. Chem. Soc., 104 (1982) 5228.
14. T.A. Early, J. Magn. Reson., 75 (1987) 129.
15. M. Alla and E. Lippmaa, Chem. Phys. Lett., 37 (1976) 260.
16. (a) E.F. Rybaczewisky, B.L. Neff, J.S. Waugh and J.S. Sherfinski, J. Chem. Phys., 67 (1977) 1231.
17. (b) G.G. Webb and K.W. Zilm, J. Am. Chem. Soc., 111 (1989) 1455.
18. N.K. Sethi, J. Magn. Reson., 94 (1991) 352.
19. D.P. Burum and A. Bielecki, J. Magn. Reson., 95 (1991) 184.
20. (a) X. Wu, S. Burns and K.W. Zilm, J. Magn. Reson., Ser. A, 111 (1994) 29.
21. (b) X. Wu and K.W. Zilm, J. Magn. Reson., Ser. A, 102 (1993) 205.
22. X.Wu and K.W. Zilm, J. Magn. Reson., Ser. A, 104 (1993) 119.
23. X. Wu, S. Zhang and X. Wu, Phys. Rev. B 37 (1988) 9827.
24. X. Wu, S. Zhang and X. W, J. Magn. Reson., 77 (1988) 343.
25. X. Wu and K.W. Zilm, J. Magn. Reson., 93 (1991) 265.
26. X. Wu, S. Zhang and X. Wu, Chem. Phys. Lett., 162 (1989) 321.
27. X. Wu and K.W. Zilm, J. Magn. Reson., Ser. A, 104 (1993) 154.
28. D.I. Hoult and R.E. Richards, J. Magn. Reson., 24 (1976) 71.
29. (a) W.T. Dixon, J. Chem. Phys., 77 (1982) 1800.
30. (b) W.T. Dixon, J. Schaefer, M.D. Scficik, E.O. Stejskal and K.A. Mckay, J. Magn. Reson., 49 (1982) 341.
31. S. Ding, C.A. McDowell and C. Ye, J. Magn. Reson., Ser. A, 109 (1994) 6.
32. (a) Z. Song, O.N. Antzutkin, X. Feng and M.H. Levitt, Solid State NMR, 2 (1993) 143.
33. (b) O.N. Antzutkin, Z. Song, X. Feng and M.H. Levitt, J. Chem. Phys., 100 (1994) 130.
34. J. Hong and G. Harbison, J. Magn. Reson., Ser. A, 105 (1993) 128.
35. J. Herzfeld and A.E. Berger, J. Chem. Phys., 73 (1980) 6021.
36. D. Fenzke, B. Maeb and H. Pfeifer, J. Magn. Reson., 88 (1990) 172.
37. J.Z. Hu, R. Fu and C. Ye, Chem. Phys. Lett., 195 (1992) 159.
38. E.T. Olejniczak, S. Vega and R.G. Griffin, J. Chem. Phys., 81 (1984) 4804.
39. D.P. Raleigh, E.T. Olejniczak and R.G. Griffin, J. Chem. Phys., 89 (1988) 1333.
40. C. Ye, B. Sun and G.E. Maciel, J. Magn. Reson., 70 (1986) 241.
41. J.Z. Hu, L. Li and C. Ye, High-field studies of argonne premium coals, in R.E. Botto and Yuzo Sanada (Eds.), Magnetic Resonances of Carbonaceous Solid, Advances in Chemistry No. 229, p. 311. American Chemical Society, Washington, DC, 1993.
42. T.M. Duncan, A Compilation of Chemical Shift Anisotropies, Farragut Press, Chicago, 1990.
43. M.S. Solum, R.J. Pugmire and D.M. Grant, Energy Fuel, 3 (1989) 187.
44. J.Z. Hu, X. Wu, N. Yang, L. Li, C. Ye, R.J. Pugmire, D.M. Grant and K. Qin, J. Magn. Reson., in preparation.
45. J.Z. Hu, A.M. Orendt, D.W. Alderman, R.J. Pugmire, C. Ye and D.M. Grant, Solid State NMR, 3 (1994) 181.
46. J.Z. Hu, M.S. Solum, R.J. Pugmire, C. Ye and D.M. Grant, Energy Fuel., 9 (1995) 717.
47. J.Z. Hu, W. Wang, F. Liu, M.S. Solum, D.W. Alderman, R.J. Pugmire and D.M. Grant, J. Magn. Reson., Ser. A, 113 (1995) 210.