Solid-state 29Si NMR analysis of amorphous silicon nitride powder

Journal of the American Ceramic Society

Volumn 79, Issue 2, 1996, Pages 513-517

  Leone, Edgar A ^a   Curran, Scan ^a   Kotun, Margaret E ^a   Carrasquillo, Gilbert ^b   Van Weeren, Remco ^b   Danforth, Stephen C ^b  

^a HONEYWELL   (United States)

^b RUTGERS UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

AMORPHOUS MATERIALS; HYDRATION; LASER APPLICATIONS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLARIZATION; POWDERS; RELAXATION PROCESSES; SYNTHESIS (CHEMICAL);

BLOCH DECAY; CROSS POLARIZATION;

SILICON NITRIDE;

EID: 0030085643     PISSN: 00027820     EISSN: None     Source Type: Journal    
DOI: 10.1111/j.1151-2916.1996.tb08156.x     Document Type: Article

References (22)

1. G. Ziegler, J. Heinrich, and G. Wötting, "Relationships between Processing, Microstructure and Properties of Dense and Reaction-Bonded Silicon Nitride," J. Mater. Sci., 22, 3041-86 (1987).
2. I. Tanaka, G. Pezzotti, T. Okamoto, Y. Miyamoto, and M. Koizumi, "Hot Isostatic Press Sintering of Silicon Nitride without Additives," J. Am. Ceram. Soc.,72 [9] 1656-60 (1989).
3. W. T. Symons and S. C. Danforth, "Hot Isostatic Pressing of Laser Synthesized Silicon Nitride Powder"; pp. 67-75 in Ceramic Materials and Components for Engines. Edited by V. J. Tennery. American Ceramic Society, Westerville, OH, 1989.
4. P. Lu, S. C. Danforth, and W. T. Symons, "Microstructure and Grain-Boundary Characterization of HIP'ed High-Purity Silicon Nitride," J. Mater. Sci., 28, 4217-22 (1993).
5. R. van Weeren, G. Carrasquillo, E. A. Leone, S. Curran, and S. C. Danforth, "Laser-Synthesized Silicon Nitride Powder: Chemical and Physical Characteristics"; pp. 47-54 in Ceramic Transactions, Vol. 42, Silicon-Based Structural Ceramics. Edited by E. W. Sheldon and S. C. Danforth. American Ceramic Society, Westerville, OH, 1994.
6. G. Ramis, G. Busca, V. Lorenzelli, M. I. Baraton, T. Merle-Mejean, and P. Quintard, "FT-IR Characterization of High Surface Area Silicon Nitride and Carbide"; pp. 173-84 in Surfaces and Interfaces of Ceramic Materials, NATO ASI Series E: Applied Sciences. Edited by L. C. Dufour, C. Monty, and G. Petot-Ervas. Kluwer Academic Publishers, Amsterdam, Netherlands, 1989.
7. P. W. Lednor, R. de Ruiter, and K. A. Emeis, "Characterization of High Surface Area Silicon Oxynitrides"; pp. 801-806 in Better Ceramics through Chemistry V, Vol. 271, Proceedings of the Materials Research Society Symposium (San Francisco, CA, 1992). Edited by M. J. Hampden-Smith, W. G. Klemperer, and C. J. Brinker. Materials Research Society, Pittsburgh, PA, 1992.
8. P. Fink, B. Müller, and G. Rudakoff, "Ammoniation and Nitridation of Highly Disperse Silica," J. Non-Cryst. Solids, 145, 99-104 (1992).
9. K. J. Nilsen, R. E. Riman, and S. C. Danforth, "The Effect of Moisture on the Processing of Silicon Nitride in Imidazoline-Hexane Solutions"; see Ref. 3, pp. 155-67.
10. 29Si-NMR Investigation of Amorphous Hydrogenated Silicon Nitride"; pp, 337-42 in Materials Issues in Amorphous-Semiconductor Technology, Vol. 70. Proceedings of the Materials Research Society Symposium. Edited by D. Adler, Y. Hamakawa, and A. Madan. Materials Research Society, Pittsburgh, PA, 1986.
11. M. D. Welch, J. Rocha, and J. Klinowski, "Characterization of Polysomatism in Biopyriboles: Double-Ariple-Chain Lamellar Intergrowths," Phys. Chem. Miner., 18, 460-68 (1992).
12. G. R. Hatfield, G. E. Maciel, O. Erbatur, and G. Erbatur, "Qualitative and Quantitative Analysis of Solid Lignin Samples by Carbon-13 Nuclear Magnetic Resonance Spectrometry," Anal. Chem.,. 59 [1] 172-79 (1987).
13. 7Li High Resolution Solid State NMR Methods," J. Non-Cryst. Solids, 107, 271-82 (1989).
14. 29Si NMR study of the Silanol Population at the Surface of Derivatized Silica," Langmuir, 6 [4] 770-75 (1990).
15. 31P MAS-NMR Study," J. Non-Cryst. Solids, 143, 21-30 (1992).
16. 2 Mixed Oxides Prepared via the Sol-Gel Process: Characterization by Spectroscopic Techniques," J. Non-Cryst. Solids, 143, 93-111 (1992).
17. H. Kaji, K. Nakanishi, N. Soga, and F. Horii, "Modification of Nanometer Range Pores in Silica Gels with Interconnected Macropores by Solvent Exchange," J. Non-Cryst. Solids, 145, 80-84 (1992).
18. 2O, as a High Surface Area Powder by Reaction of Silica with Ammonia at 1100°C," J. Chem. Soc., Chem. Commun., [5] 320-21 (1989).
19. H.-P. Baldus, W. Schnick, J. Lücke, U. Wannagat, and G. Bogedain, "Silicon Phosphorus Nitride, the First Ternary Compound in the Silicon-Phosphorus-Nitrogen System," Chem. Mater., 5 [6] 845-50 (1993).
20. K. R. Carduner, R. O. Carter III, M. E. Milberg, and G. M. Crosbie, "Determination of Phase Composition of Silicon Nitride Powders by Silicon-29 Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy," Anal. Chem., 59 [23] 2794-97 (1987).
21. 29Si NMR Characterization of α- and β-Silicon Nitride," J. Am. Chem. Soc., 112 [12] 4676-79 (1990).
22. 15N-Enriched Silicon Nitrides," Chem. Mater., 2 [3] 320-23 (1990).