27Al nuclear magnetic resonance of glassy and crystalline Zr(1-x)AlxO(2-x/2) materials prepared from solution precursors

Journal of the American Ceramic Society

Volumn 79, Issue 2, 1996, Pages 321-326

  Balmer, Mari Lou ^a,b   Eckert, Hellmut ^a,c   Das, Nandini ^a   Lange, Fred F ^a  

^a UNIVERSITY OF CALIFORNIA   (United States)

^b PACIFIC NORTHWEST NATIONAL LABORATORY   (United States)

^c UNIVERSITY OF MÜNSTER   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

ALUMINA; ALUMINUM; AMORPHOUS MATERIALS; COMPOSITION EFFECTS; CRYSTAL ATOMIC STRUCTURE; CRYSTALLINE MATERIALS; CRYSTALLIZATION; DIFFUSION IN SOLIDS; MATHEMATICAL MODELS; NUCLEAR MAGNETIC RESONANCE; ZIRCONIUM COMPOUNDS;

MAGIC ANGLE SPINNING NUCLEAR MAGNETIC RESONANCE (MAS NMR); SOLUTION PRECURSORS;

SOLID SOLUTIONS;

EID: 0030082621     PISSN: 00027820     EISSN: None     Source Type: Journal    
DOI: 10.1111/j.1151-2916.1996.tb08123.x     Document Type: Article

References (22)

1. (2-x/2) Materials Synthesized with Liquid Precursors," J. Am. Ceram. Soc., 77 [8] 2069-75 (1994).
2. 3 via the Solution Precursor Method," J. Am. Ceram. Soc., 78 [6] 1489-94 (1995).
3. L. J. Alvarez and J. F. Sanz, "Molecular Dynamics Study of the Structure of γ-Alumina," Chem. Phys. Lett., 192 [5,6] 463-68 (1992).
4. T. E. Wood, A. R. Siedle, J. R. Hill, R. P. Skarjune, and C. J. Goodbrake, "Hydrolysis of Aluminum-Are All Gels Created Equal?" Mater. Res. Soc. Symp. Proc., 180, 97-116 (1992).
5. 27Al MAS NMR Studies of a New Polyoxyaluminum Cluster and Its Selective Transformation to Five-Coordinate Aluminum in the Solid State," J. Chem. Soc., Chem. Commun., 251-53 (1992).
6. D. Coster and J. J. Fripiat, "Memory Effects in Gel-Solid Transformation in Coordinately Unsaturated Al Sites in Nano-Sized Aluminas," Chem. Mater., 5, 1204-10 (1993).
7. I. Farnan, R. Dupree, Z. Jeong, G. E. Thompson, G. C. Wood, and A. J. Forty, "Structural Chemistry of Anodic Alumina," Thin Solid Films, 173, 209-15 (1989).
8. 3 Glasses," J. Phys. Chem., 95, 4483 (1991).
9. 3 System via Raman and Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy," Phys. Chem. Glasses, 32, 149-56 (1991).
10. 27Al MAS-NMR Investigation," J. Am. Ceram. Soc., 74 [10] 2398-403 (1991).
11. 29Si NMR Study of Sol-Gel-Derived Aluminosilicates and Sodium Aluminosilicates," J. Mater. Sci., 23, 2908-12 (1988).
12. 29Si MAS NMR," J. Am. Ceram. Soc., 73 [12] 3663-69 (1990).
13. A. Yasumori, M. Iwasaki, H. Karazoe, and M. Yamane, "Nuclear Magnetic Resonance Study of the Structure of Aluminosilicate Gel and Glass," Phys. Chem. Glasses, 31, 1-9 (1990).
14. 27Al Magic Angle Spinning Nuclear Magnetic Resonance," Phys. Chem. Glasses, 33, 73-78 (1992).
15. 3 Glasses," J. Am. Ceram. Soc., 70 [1] C-10-C-12 (1987).
16. 3 Glasses: An NMR and XPS Study," J. Am. Ceram. Soc., 73 [8] 2293-300 (1990).
17. 27Al during the Devitrification of an Aluminoborate Glass," Phys. Chem. Glasses, 26, 50-52 (1985).
18. L. B. Alemany and G. W. Kirker, "First Observation of 5-Coordinate Aluminum by MAS NMR in Well-Characterized Solids," J. Am. Ceram. Soc., 108, 6158-62 (1986) and references sited therein.
19. B. C. Bunker, R. J. Kirkpatrick, and R. K. Brow, "Local Structure of Alkaline-Earth Boroaluminate Crystals and Glasses: I, Crystal Concepts-Structural Predictions and Comparisons to Known Crystal Structures," J. Am. Ceram. Soc., 74 [6] 1425-29 (1991).
20. 27Al MAS NMR Spectroscopy of Alkaline-Earth Boroaluminate Glasses," J. Am. Ceram. Soc., 74 [6] 1430-38 (1991).
21. 2 and Its Effect on Grain Growth," Acta Metall., 42 [6] 1829-46 (1994).
22. E. E. Underwood, "Applications of Quantitative Metallography"; pp. 37-47 in Metals Handbook, Vol. 8, Metallography, Structures, and Phase Diagrams. American Society for Metals, Metals Park, OH, 1973.